A kind of weakly cross-linked granular control and drive agent for enhancing oil recovery and its preparation method
A recovery factor and flood control agent technology, which is applied in the field of weakly cross-linked particle control and flooding agent and its preparation, can solve the problems of poor adaptability to heterogeneous formations, decreased viscosity, high cross-linking degree, etc., and achieve a dense cross-linked network structure , improved aging resistance, simple synthesis method
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Embodiment 1
[0025] Dissolve 25 parts of acrylamide in 62 parts of water to make a solution, dissolve 0.05 part of dimethylaminoethyl methacrylate in 8 parts of water to make a solution, and dissolve 0.00025 parts of polyethylene glycol diacrylate in 5 parts of water to make a solution , added to the three-necked flask in turn, and placed in a water bath at 15°C; after passing through nitrogen for 30 minutes, a solution prepared by dissolving 0.0025 parts of ammonium persulfate in 12 parts of water was added to the three-necked flask. After the temperature rise of the reaction solution is greater than 1°C, stop the nitrogen flow. After the reaction, put the three-neck bottle in a 75°C water bath to keep warm for 4 hours, then take out the gel, cut it into pieces, dry it, crush it, and sieve it. Powdered product available.
Embodiment 2
[0027] Dissolve 50 parts of acrylamide in 100 parts of water to make a solution, dissolve 0.15 parts of dimethylaminoethyl methacrylate in 20 parts of water to make a solution, and dissolve 0.00025 parts of polyethylene glycol diacrylate in 15 parts of water to make a solution , added to the three-necked flask in turn, and placed in a water bath at 12°C; after passing through nitrogen for 30 minutes, a solution prepared by dissolving 0.01 parts of ammonium persulfate in 25 parts of water was added to the three-necked flask. After the temperature rise of the reaction solution is greater than 1°C, stop the nitrogen flow. After the reaction, put the three-neck bottle in a 70°C water bath to keep warm for 6 hours, then take out the gel, cut it into pieces, dry it, crush it, and sieve it. Powdered product available.
Embodiment 3
[0029] Dissolve 100 parts of acrylamide in 250 parts of water to make a solution, dissolve 0.4 parts of dimethylaminoethyl methacrylate in 40 parts of water to make a solution, and dissolve 0.0008 parts of polyethylene glycol diacrylate in 20 parts of water to make a solution , into the three-necked flask in turn, and placed in a water bath at 12°C; after 30 minutes of nitrogen gas, a solution prepared by dissolving 0.02 parts of ammonium persulfate in 30 parts of water was added to the three-necked flask. When the temperature rise of the reaction solution is greater than 1°C, stop the nitrogen flow. After the reaction, put the three-neck bottle into an 80°C water bath to keep warm for 3 hours, then take out the gel, cut it into pieces, dry it, crush it, and sieve it. Powdered product available.
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