A kind of synthesis of perylene imide derivative and preparation method of micron wire
A technology of perylene imide and synthesis method, which is applied in the field of synthesis of perylene imide derivatives and preparation of micron wires, can solve the problems that have not been reported, and achieve the effect of high product purity, less by-products, and simple synthesis method
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[0022] The present invention is further illustrated by the following examples.
[0023] The synthetic method of described perylene imide derivative:
[0024] 1-NO 2 -3,4; 9,10-perylenetetracarboxylic acid diimide (0.6g, 1mmol) was dissolved in 60mL of N-methylpyrrolidone, under vigorous stirring, heated at 180°C for 5 hours, and the reacted solution After cooling, drop it into 500mL hydrochloric acid solution with a concentration of 2moL / L to precipitate precipitates, vacuum filter the precipitates, wash the solids with distilled water, and dry them in vacuum. phase, purified by silica gel column chromatography to obtain 0.34 g of a bright yellow solid product with a yield of 60%. 1 H-NMR (CHCl 3 , TMS, ppm): δ=8.95 (d, 2H), 8.83 (d, 4H), 5.16 (m, 2H), 2.66-2.63 (m, 4H), 1.94-1.55 (m, 8H), 1.41-1.26 (m, 8H). 13 C NMR (75MHz, CDCl 3 , ppm): δ=164.78, 163.74, 154.15, 133.93, 130.38, 126.46, 125.03, 124.36, 119.34, 54.50, 29.27, 26.65, 25.48.FT-IR (KBr, cm -1 ): v=2922, 16...
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