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Preparation technology of discolored aqueous chilli extract

A capsicum extract, water-based technology, applied in the field of preparation of decolorized water-based capsicum extract, can solve the problems of complicated operation, low yield, large solvent consumption, etc., and achieve the effect of small loss, high yield, and low cost

Inactive Publication Date: 2016-02-10
丁春燕
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

But the above method exists, a large amount of capsanthin cannot be recovered, the solvent consumption is large, the decolorization effect is not good, the adsorbent cannot be recycled, and it is difficult to large-scale industrial production
[0003] In the method of refining capsicum essence by using macroporous resin, Chinese patents CN1392201A and CN101940289A use macroporous resin to separate capsicum essence, which has large solvent consumption, complicated operation and low yield, and cannot be fully applied to the production of decolorized capsicum essence.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] The crude capsicum extract (capsaicin content is 31%, color value is 10E) 5kg is stirred and dissolved in 50L isopropanol at 45°C, and allowed to settle for 4.5 hours; , under the vacuum degree of 0.07MPa, recover the isopropanol to 10L; put 10L of concentrated solution into the reflux decolorization tank, add 0.6kg of decolorizing resin D900, reflux and decolorize at a temperature of 85 ° C for 1 hour, filter, concentrate under reduced pressure and recover Isopropyl alcohol, desolventized to obtain 2.29kg of decolorized capsicum extract (capsaicin content is 63%, color value is 0.5E); according to the product standard with capsaicin content of 3.3%, 2.29kg of decolorized capsicum extract is transferred to Put it into the mixing tank, add 7.5kg of Tween 80 and monoglyceride compound food emulsifier, fully dissolve it, add water to 43.7kg, and prepare 3.3% decolorized water-based capsicum essence.

[0021] Capsaicin content of decolorized water-based capsaicin: 3.31%.

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Embodiment 2

[0025] 5.5kg of the crude capsicum extract (capsaicin content is 28.8%, color value is 12E) is stirred and dissolved in 50L of ethanol at 45°C, and allowed to settle for 5 hours; Under the vacuum degree of 0.07MPa, ethanol was recovered to 10L; 10L of the concentrated solution was poured into the reflux decolorization tank, 0.5kg of decolorizing resin D900 was added, refluxed and decolorized at a temperature of 80 ° C for 1 hour, filtered, concentrated under reduced pressure to recover ethanol, and decolorized. Dissolve to obtain 2.5kg of decolorized capsicum extract (capsaicin content is 61.8%, color value is 0.63E); according to the product standard of capsaicin content of 6.6%, 2.42kg of decolorized capsicum extract is transferred into the blending tank , add 6kg of polyglycerol ester and monoglyceride compound food emulsifier, fully dissolve and add water to 22.7kg, and prepare 6.6% decolorized water-based capsaicin.

[0026] Capsaicin content of decolorized water-based ca...

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PUM

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Abstract

The invention relates to a production technology of discolored aqueous chilli extract. The production technology comprises the following steps: step one, dissolving a crude product of chilli extract into alcohol, stirring to dissolve the crude product at a certain temperature, and then carrying out settlement; step two, collecting supernate obtained in the step one, and condensing the supernate until one fifth of the supernate is left; step three, adding a certain amount of discoloring resin into the concentrated supernate obtained in the step two to discolor the supernate; step four, filtering the concentrated supernate, condensing the filtrate, recovering the solvent, desolventizing the concentrated supernate to obtain qualified discolored chilli extract; step five, adding a certain amount of emulsifying agent into the chilli extract to carry out emulsification, and blending to obtain discolored aqueous chilli extract with a certain concentration. The produced discolored aqueous chilli extract has the advantages of high solubility, low color value, and no impurity or precipitate, has a light yellow color, and is transparent. The application range of chilli extract is enlarged. The capsaicin content of the produced discolored aqueous chilli extract is 1 to 18%.

Description

technical field [0001] The invention belongs to the field of preparation of natural pigments, and in particular relates to a preparation process of decolorized water-based capsaicin. Background technique [0002] In the current process for producing decolorized capsaicin, activated carbon or diatomaceous earth, activated clay, hydrogen peroxide, etc. are often used for decolorization. But the above method exists, a large amount of capsanthin cannot be recovered, the solvent consumption is large, the decolorization effect is not good, the adsorbent cannot be recycled, and it is difficult to large-scale industrial production. [0003] In the method of using macroporous resin to purify capsicum essence, Chinese patents CN1392201A and CN101940289A utilize macroporous resin to separate capsicum essence, which has large solvent consumption, complicated operation and low yield, which cannot be fully applied to the production of decolorized capsicum essence. SUMMARY OF THE INVENTI...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/226A23L1/27
Inventor 丁春燕
Owner 丁春燕
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