A kind of special sepiolite fiber for papermaking and preparation method thereof
A technology of sepiolite fiber and sepiolite, which is applied in the directions of fiber processing, textile and papermaking, physical processing, etc., can solve the adverse effects of paper performance and strength indicators, difficulty in exerting fiber network support, and reduced paper sheet strength properties. and other problems to achieve the effect of increasing the number, increasing the softness, increasing the strength and toughness
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Embodiment 1
[0025] (1) adding 10 parts by weight of carbon nanotubes into a 40% sulfuric acid solution and stirring for 2 to 3 h, washing until the solution is 5 to 7, filtering and drying to obtain acidified carbon nanotubes;
[0026] (2) Make 70 parts by weight of sepiolite fibers with layered fibers into a pulp concentration of 10%, soak for 24 h, add the acidic carbon nanotubes obtained in step (1), and add 8 parts by weight of hexametaphosphoric acid Sodium, use ultrasonic wave to disperse for 30~40min, and get modified sepiolite fiber by centrifugal filtration;
[0027] (3) Put the modified sepiolite fibers obtained in step (2) and 10 parts by weight of β-cyclodextrin into the plasma equipment, set the power at 80 W, the pressure at 30 Pa, and discharge for 5 min to obtain Cyclodextrin-modified sepiolite fibers were added to cetyltrimethylammonium bromide solution with a mass fraction of 10%, and stirred and mixed for 10-20 min to make the cationic surfactant cetyltrimethylammonium ...
Embodiment 2
[0029] (1) adding 10 parts by weight of carbon nanotubes into a sulfuric acid solution with a concentration of 40% and stirring for 2-3 h, washing until the solution is 5-7, filtering and drying to obtain acidified carbon nanotubes;
[0030] (2) Prepare 70 parts by weight of sepiolite fibers with layered fibers to a pulp concentration of 10%, soak for 24 hours, add the acidic carbon nanotubes obtained in step (1), and add 8 parts by weight of polyphosphoric acid Sodium, use ultrasonic wave to disperse for 30~40min, and get modified sepiolite fiber by centrifugal filtration;
[0031](3) Put the modified sepiolite fiber obtained in step (2) and 20 parts by weight of carboxymethyl β-cyclodextrin into the plasma equipment, set the power at 80 W, the pressure at 20 Pa, and discharge for 10 min to obtain cyclodextrin-modified sepiolite fibers, which were added to cetyltrimethylammonium bromide solution with a mass fraction of 20%, and stirred and mixed for 10-20 min to make the cati...
Embodiment 3
[0033] (1) adding 20 parts by weight of carbon nanotubes into a sulfuric acid solution with a concentration of 60% and stirring for 2-3 h, washing until the solution is 5-7, filtering and drying to obtain acidified carbon nanotubes;
[0034] (2) Make 60 parts by weight of sepiolite fibers with layered fibers into a pulp concentration of 5%, soak for 24 h, add the acidic carbon nanotubes obtained in step (1), and add 5 parts by weight of sodium triphosphate , use ultrasonic wave to disperse for 30~40min, and obtain modified sepiolite fiber by centrifugal filtration;
[0035] (3) Put the modified sepiolite fiber obtained in step (2) and 10 parts by weight of methyl β-cyclodextrin into the plasma equipment, set the power at 80 W, the pressure at 20 Pa, and discharge for 10 min , to obtain cyclodextrin-modified sepiolite fiber, add it to cetyltrimethylammonium bromide solution with a mass fraction of 10%, and stir and mix for 10~20 min to make the cationic surfactant cetyltrimethy...
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