A kind of micro-smoke type three-color fireworks drug granule and its application
A technology of three primary colors and fireworks, which is applied in the field of fireworks medicine, can solve the problems of cumbersome formula design, low production efficiency, and difficulty in standardization, and achieve simplification and standardization of production links, less smoke production, and easy control of quality stability Effect
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[0033] A preparation method of micro-smoke type three-color fireworks drug granules, comprising the following steps: dissolving nitrocellulose or smokeless powder containing nitrocellulose into a solvent to obtain a sol containing nitrocellulose, emulsifying the sol into an aqueous solution of dyeing agent, and then Disperse the obtained emulsion again into an aqueous solution of the same type and concentration as the above-mentioned dye solution to disperse into balls. The emulsion is dispersed into spherical droplets, followed by solvent removal and material separation to obtain a spherical solution containing nitrocellulose and dye aqueous solution. The granules are dried to obtain smoky three-color fireworks drug granules. The type and concentration of the aqueous dye solution added in the emulsification process and the dispersion into ball process are the same. Strontium nitrate, copper chloride, barium chloride and barium nitrate are selected as the dyeing agent, the red...
Embodiment 1
[0045] Use single-base waste powder with a nitrocellulose content greater than 85% as the raw material, add it to the molding equipment, add ethyl acetate solvent 10 times the weight of the single-base waste powder under stirring, and stir and dissolve at 45°C-50°C 30-60min, form polymer sol; Carry out emulsification and foaming operation under stirring state, add mass concentration in this step and be the cupric chloride aqueous solution of 5%, the amount of the cupric chloride aqueous solution that adds is the quality of single base waste powder 6 times, and then continue to stir at 50-60°C for 30min-60min, the polymer sol forms an emulsion, when the system temperature is adjusted to 65°C-68°C, add 12 times the mass of single-base waste powder containing dispersant and 5 % copper chloride aqueous solution is added to the system to disperse into balls, gelatin is used as a dispersant, and the amount of dispersant added is 0.5% of the total mass of water. Continue to maintain ...
Embodiment 2
[0052] Using the same process as in Example 1, adopting single-base waste gunpowder with a nitrocellulose content greater than 85% as a raw material, using strontium nitrate as a dyeing agent, the concentration of the strontium nitrate solution used in the emulsification foaming and ball forming medium is all 5%. .
[0053] Performance parameters:
[0054]
[0055] With the color value T as the abscissa and the relative intensity I as the ordinate, use IMAGE-PRO software to analyze the color components of the flame picture into a two-dimensional curve as Image 6 (R in the figure represents the red component, G represents the green component, and B represents the blue component) for intuitive analysis and color characterization.
[0056] By flame picture ( Figure 5 ) It can be clearly seen that the flame is red and has high purity, which can meet the performance requirements of the base color medicine. from Image 6 According to the analysis, the relative intensity of ...
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