Preparation method and equipment of fully water-soluble high imino partially methylated amino resin

An amino resin and water-soluble technology, applied in chemical instruments and methods, chemical/physical processes, chemical/physical/physical-chemical processes, etc., can solve the problems of saturation phenomenon, poor shock isolation effect, etc., and achieve convenient wiring, Good shock isolation effect and high mixing efficiency

Active Publication Date: 2017-11-07
ZHEJIANG XINHUA NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The invention provides a method for preparing a fully water-soluble high-imino partially methylated amino resin that will not produce saturation when dissolved in water, and solves the problem of water-soluble resins prepared by the existing method being dissolved in water. problem with saturation
[0005] The invention also improves a kind of water-soluble high imino partly methylated amino resin preparation equipment with large reversing range, good shock isolation effect and the ability to change the height of the stirring blade according to the change of the height of the material in the container, which solves the existing reaction If the direction of the feed port of the kettle cannot be adjusted to the same direction as the direction of the feed pipe, it is necessary to make an elbow to change the direction, and it is impossible to efficiently stir the material when the height of the material changes without producing stirring blades. Problems of idle phenomenon and poor vibration isolation effect

Method used

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  • Preparation method and equipment of fully water-soluble high imino partially methylated amino resin
  • Preparation method and equipment of fully water-soluble high imino partially methylated amino resin
  • Preparation method and equipment of fully water-soluble high imino partially methylated amino resin

Examples

Experimental program
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Effect test

Embodiment 1

[0047] Embodiment one, see figure 1 , a water-soluble high imino partially methylated amino resin preparation equipment, including a container 1, a reversing tube 2, a tightening bolt 24 and a stirrer 5.

[0048] The container 1 is provided with a feed opening 12 .

[0049] The reversing pipe 2 is butted on the inlet end of the feed port 12 . The reversing pipe 2 is affixed together with the feed port 12 by tightening bolts 24 .

[0050] The agitator 5 includes a rotating shaft 51 , a stirring blade 52 , a motor 53 , a driving gear 54 and a driven gear 55 . The rotating shaft 51 is input into the container 1 . The rotating shaft 51 is rotatably connected to the container 1 . The rotating shaft 51 extends in the vertical direction. The stirring blade 52 is connected to the part of the rotating shaft 51 located in the container. The stirring blade 52 is a blade structure. The driven gear 55 is fixed on the upper end of the rotating shaft 51, and the driven gear 55 and the...

Embodiment 2

[0058] Embodiment two, the difference with embodiment one lies in the change of the structure of the preparation equipment of the water-soluble high imino part methylated amino resin, specifically changed as follows:

[0059] see Figure 6 , The shock-isolation foot 9 is also provided with a driving mechanism 6 . The inner ring 922 is rotatably connected to the rubber ring 7 , and the rubber ring 7 is fixedly connected with the connecting ring 921 .

[0060]The drive mechanism 6 includes a ratchet 61 , a pawl 62 for driving the ratchet, and a drive rod 63 . The ratchet 61 is coaxially connected with the inner ring 922 . The ratchet 61 is integrated with the inner ring 922 . The pawl 62 is fixedly connected to one end of the driving rod 63 . The upper section 92 is provided with a sliding hole 924 . The other end of the driving rod 63 can slide through the sliding hole 924 two-dimensionally. The lower end of the drive rod 63 is slidably hooked to the lower section 91 alon...

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Abstract

The invention relates to the technical field of amino resin production, provides a method capable of preparing full-water-soluble high-imino partial-methylated amino resin which cannot be saturated when the resin is dissolved in water in order to solve the problem that a saturation phenomenon can be produced when the water-soluble resin is dissolved in water, provides equipment which is used for preparing the full-water-soluble high-imino partial-methylated amino resin, has a wide reversing range and good shock insulation effect and can change height of stirring blades according to height change of a material in a container, and solves the problems that a bend is required to be manufactured for reversing under the condition that a direction of a reaction kettle at a feed port and a trend of a feed pipe cannot be adjusted to the same, efficient material stirring and avoidance of a stirring blade idling phenomenon cannot be realized simultaneously during the height change of the material and the shock insulation effect is poor. The preparation equipment comprises the container and a stirrer, wherein the container is provided with shock insulation legs and the feed port adjustable in the feeding direction, the height of each stirring blade of the stirrer is adjustable, and a motor is provided with a terminal.

Description

technical field [0001] The invention relates to the technical field of amino resin production, in particular to a preparation method and equipment for fully water-soluble high imino partially methylated amino resin. Background technique [0002] Water-soluble amino resins are the future development direction of amino resin crosslinking agents. Water is used as a solvent to replace the original organic solvents such as alcohols, which is a huge improvement in terms of environmental protection. At present, countries such as Europe and the United States have banned the use of solvent-based coatings. Although my country's coating industry is still dominated by solvent-based coatings, it is also actively developing towards water-based coatings in recent years. For the future coatings market, water-based coatings are an inevitable trend, and fully water-soluble amino resins that match water-based coatings will inevitably become the main body of amino resin crosslinking agents in t...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08G12/42B01J19/18
CPCB01J19/0053B01J19/18C08G12/427
Inventor 王正强谌兴旺祝晋文
Owner ZHEJIANG XINHUA NEW MATERIAL TECH CO LTD
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