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Identification method of white fresh bark in Fengshining medicinal wine

A technology of Fengshi Ning medicine and white fresh skin, applied in the direction of measuring devices, instruments, scientific instruments, etc., to achieve high controllability, scientific and effective identification, and the effect of improving quality inspection standards

Active Publication Date: 2018-08-21
GUIZHOU XINBANG PHARMACEUTICAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing quality standard of Fengshining medicinal wine does not involve the identification of white fresh skin. Therefore, it is particularly important to study a method that can efficiently and accurately identify white fresh peel in Fengshining medicinal wine, which is beneficial to the quality detection of Fengshining medicinal wine. necessary

Method used

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  • Identification method of white fresh bark in Fengshining medicinal wine
  • Identification method of white fresh bark in Fengshining medicinal wine
  • Identification method of white fresh bark in Fengshining medicinal wine

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0041] The identification method of white fresh skin in Fengshining medicinal wine comprises the following steps:

[0042] (1) Preparation of the test solution: Take 45 mL of this product, add 20 mL of ethyl acetate, shake and extract once to obtain ethyl acetate liquid, evaporate to dryness, add 1 mL of methanol to the residue to dissolve it, and use it as the test solution;

[0043] (2) Preparation of reference substance solution: get phellodendron reference substance and alkone reference substance, add methanol to make a mixed solution containing 1 mg phellodendron reference substance and 1 mg alkone reference substance in every 1 mL, as the reference substance solution;

[0044] (3) Identification: According to the "Chinese Pharmacopoeia" 2015 edition four general rules 0502 thin-layer chromatography test, absorb 4 μL of the reference substance solution and 8 μL of the test solution, respectively spot on the same silica gel G thin-layer plate, and use toluene-cyclohexane -...

Embodiment 2

[0046] The identification method of white fresh skin in Fengshining medicinal wine comprises the following steps:

[0047] (1) Preparation of the test solution: take 55mL of this product, add 20mL, 25mL, and 30mL of ethyl acetate respectively, shake and extract 3 times, combine the ethyl acetate solution, evaporate to dryness, add 2mL of methanol to the residue to dissolve it, and use it as The test solution;

[0048] (2) Preparation of reference substance solution: get phellodendron reference substance and alkone reference substance, add methanol to make a mixed solution containing 1 mg phellodendron reference substance and 1 mg alkone reference substance in every 1 mL, as the reference substance solution;

[0049] (3) Identification: According to the "Chinese Pharmacopoeia" 2015 edition four general rules 0502 thin-layer chromatography test, absorb 8 μL of the reference substance solution and 12 μL of the test solution, respectively spot on the same silica gel G thin-layer p...

Embodiment 3

[0051] The identification method of white fresh skin in Fengshining medicinal wine comprises the following steps:

[0052] (1) Preparation of the test solution: Take 50 mL of this product, add 20 mL and 30 mL of ethyl acetate respectively, shake and extract twice, combine the ethyl acetate solution, evaporate to dryness, add 1 mL of methanol to the residue to dissolve it, and use it as the test solution. product solution;

[0053] (2) Preparation of reference substance solution: get phellodendron reference substance and alkone reference substance, add methanol to make a mixed solution containing 1 mg phellodendron reference substance and 1 mg alkone reference substance in every 1 mL, as the reference substance solution;

[0054] (3) Identification: According to the "Chinese Pharmacopoeia" 2015 edition four general rules 0502 thin-layer chromatography test, absorb 5 μL of the reference substance solution and 10 μL of the test solution, respectively spot on the same silica gel G...

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Abstract

The invention discloses an identification method of cortex dictamni in anti-rheumatism medicinal liquor. The method is a thin-layer chromatography method by using an obakunone reference substance and a fraxinellone reference substance as control and using toluene-cyclohexane-ethyl acetate as a developing solvent, wherein the ratio of toluene to cyclohexane to ethyl acetate is 2-8: 2-6: 2-6. By the identification method of cortex dictamni in anti-rheumatism medicinal liquor, cortex dictamni in anti-rheumatism medicinal liquor can be efficiently and accurately identified. The method has higher controllability, is simple to operate, has high separation degree and good reappearance, has no interference with negative control, and will not be influenced by thin layer plates from different manufacturers and temperature and humidity conditions. According to the identification method, cortex dictamni component in anti-rheumatism medicinal liquor can be identified accurately, comprehensively, scientifically and effectively. Quality detection standard is raised, and stability, safety and effectiveness of product quality are further ensured.

Description

technical field [0001] The invention relates to a method for identifying white fresh bark in Fengshining medicated wine, and specifically belongs to the technical field of traditional Chinese medicine detection. Background technique [0002] Fengshining Medicinal Wine is made from Spatholobus Polygoni Multiflori, Radix Polygoni Multiflori, Herbs, Bran Stir-fried Atractylodes, Sarsaparilla, Geranium, Safflower, Black Snake, Wujiapi, Guizhi, Silkworm Sand, and Bai Xian Bark, Shichangpu, Sophora flavescens, Asarum, Xugufeng, Galangal, Sangzhi, Angelica dahurica, Rehmannia glutinosa, Xanthium and Chuanxiong. Function is expelling wind and activating blood circulation, promoting dampness and dredging collaterals. In the prescription, Caulis Spatholobus is the monarch drug, which has the effects of promoting blood circulation and dredging collaterals, eliminating phlegm and promoting regeneration, and fluent meridians. The minister uses fleece-flower root, rehmannia glutinosa, a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90
CPCG01N30/90
Inventor 罗治桃
Owner GUIZHOU XINBANG PHARMACEUTICAL CO LTD
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