Kaki calyx extract and application thereof

A technique for extracting and persimmon stalks, applied in the field of natural product chemistry

Active Publication Date: 2017-02-15
ANHUI UNIVERSITY OF TRADITIONAL CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, there is no research and application about persimmon stal

Method used

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  • Kaki calyx extract and application thereof
  • Kaki calyx extract and application thereof
  • Kaki calyx extract and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] Embodiment 1: the concentration of extraction solvent (ethanol) is selected

[0017] 1. Take 10 g of the dried and pulverized powder of persimmon stems and leaves, soak it with 100 ml of pure water at room temperature and ultrasonically extract it twice, each time for 60 minutes (500 W), combine the filtrate after filtration, recover the solvent under reduced pressure until dry, and obtain crude persimmon pedicles. Extract; take the obtained persimmon pedicle crude extract and prepare a 0.05mg / ml solution for later use.

[0018] 2. Take 10 g of the dried and pulverized powder of persimmon stalks and leaves, soak it with 100 ml of ethanol solution with a volume concentration of 30% at room temperature and extract it ultrasonically twice, each time for 60 min (500 W). After filtering, combine the filtrates, and recover the solvent under reduced pressure to dryness. , to obtain the crude extract of persimmon pedicle; take the obtained crude persimmon pedicle extract and pr...

Embodiment 2

[0033] Embodiment 2: the selection of solid-liquid ratio

[0034] 1. Take 10 g of the dried and pulverized powder of persimmon stalks and leaves, soak it with 80 ml of ethanol solution with a volume concentration of 60% at room temperature and extract it twice with ultrasound, each time for 60 min (500 W). After filtering, combine the filtrates, and recover the solvent under reduced pressure to dryness. , to obtain the crude extract of persimmon pedicle; take the obtained crude persimmon pedicle extract and prepare a 0.05mg / ml solution for later use.

[0035] 2. Take 10 g of the dried and pulverized powder of persimmon stalks and leaves, soak it with 100 ml of ethanol solution with a volume concentration of 60% at room temperature and extract it twice with ultrasound, each time for 60 min (500 W). After filtering, combine the filtrates and recover the solvent under reduced pressure to dryness. , to obtain the crude extract of persimmon pedicle; take the obtained crude persimmo...

Embodiment 3

[0042] Embodiment 3: the preparation of persimmon pedicle extract

[0043] The preparation of crude extract of persimmon stalks: take 10 g of dried and pulverized powder of persimmon stalks and leaves, immerse at room temperature with 120 ml of ethanol solution with a volume concentration of 60%, and ultrasonically extract 2 times, each time for 60 min (500 W), filter and combine the filtrates, The solvent was recovered under reduced pressure to dryness, and the crude extract of persimmon stalks was obtained for efficacy research.

[0044] Preparation of persimmon pedicle activity-enriched extract: Get 100 g of dried and pulverized powder of persimmon pedicle stem and leaf, soak it with 1200 ml of ethanol solution with a volume concentration of 60% at room temperature and extract it twice by ultrasonic, each time for 60 min (500 W), and combine the filtrate ( About 2200ml), the solvent is recovered under reduced pressure until there is no alcohol smell, passed through D101 res...

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PUM

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Abstract

The invention discloses a kaki calyx extract and an application thereof. The kaki calyx extract is obtained by extracting the raw material kaki calyx. The kaki calyx extract disclosed by the invention has perfect whitening and anti-aging functions and can be applied to the fields of skincare products, healthcare food and medicine and particularly to the skincare products.

Description

technical field [0001] The invention relates to a persimmon pedicle extract and its application, belonging to the field of natural product chemistry. Background technique [0002] Persimmon pedicle is the dry persistent calyx of Diospyros kaki (Diospyros kaki), a traditional Chinese medicine mainly produced in Hebei, Henan, Shandong, Fujian and other places. It is bitter, warm in nature, has the function of lowering Qi and stopping hiccups, and is often used for hiccups caused by stomach cold and Qi stagnation. "Compendium of Materia Medica" records: "The ancient prescription only uses persimmon stalks to boil juice and drink it, whichever is bitter and warm can reduce adverse qi." "Jisheng" persimmon stalks powder is added with the pungent heat of cloves and ginger to open phlegm and relieve depression. However, what people used in the past is effective.” Modern pharmacological studies have shown that persimmon pedicle extracts also have sedative, antiarrhythmic and certai...

Claims

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Application Information

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IPC IPC(8): A61K8/9789A61Q19/08A61Q19/02A61K36/44A61P17/00A23L33/105
CPCA23V2002/00A61K8/97A61K36/44A61K2236/33A61K2236/333A61K2236/55A61Q19/02A61Q19/08A23V2250/21A23V2200/302A23V2200/318
Inventor 王国凯刘劲松孙云鹏刘松照郁阳
Owner ANHUI UNIVERSITY OF TRADITIONAL CHINESE MEDICINE
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