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A kind of preparation method of antibacterial interior wall nano-emulsion paint

A latex paint and nano technology, applied in the field of paint, can solve the problems of mold on the interior wall, long wet weather, and bacterial growth on the wall.

Active Publication Date: 2019-05-17
上海流丹新型材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to provide a preparation method of antibacterial interior wall nano-emulsion paint, which aims to solve the problem of bacterial growth on the wall surface in the living room and the problem of mildew on the interior wall caused by long humid weather

Method used

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  • A kind of preparation method of antibacterial interior wall nano-emulsion paint

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Embodiment 1: a kind of preparation method of antibacterial interior wall nano-emulsion paint,

[0028] Step 1, solution A: Dissolve 8 parts of tetrabutyl titanate in a mixed solution of 5 parts of absolute ethanol and 5 parts of acetic acid, and fully stir for 20 minutes;

[0029] Solution B: Dissolve 2 parts of acetylacetone and 5 parts of absolute ethanol and mix with 5 parts of anhydrous acetic acid under stirring conditions, add 2.4 parts of mineral oil and 0.1 part of silver nitrate, mix well, and fully stir for 12 hours;

[0030] Step 2, mix A solution and B solution according to the ratio of 1:1, and fully stir for 12 hours to obtain a precursor colloid solution for preparing silver / titanium dioxide nanotubes;

[0031] Step 3, put the precursor solution prepared in step 2 into a spinneret with an inner diameter of 1 mm, the receiving device is grounded and rotated directly as a 100 mm aluminum roller, the receiving distance is 18 cm, the spinning voltage is 15 k...

Embodiment 2

[0036] Embodiment 2: a kind of preparation method of antibacterial interior wall nano-emulsion paint,

[0037] Step 1, solution A: dissolve 10 parts of tetrabutyl titanate in a mixed solution of 10 parts of absolute ethanol and 8 parts of acetic acid, and fully stir for 12 hours;

[0038] Solution B: Dissolve 6 parts of acetylacetone and 10 parts of absolute ethanol and mix with 7 parts of anhydrous acetic acid under stirring conditions, add 2.4 parts of mineral oil and 0.1 part of silver nitrate, mix well, and fully stir for 12 hours;

[0039] Step 2, mix A solution and B solution according to the ratio of 1:1, and fully stir for 12 hours to obtain a precursor colloid solution for preparing silver / titanium dioxide nanotubes;

[0040] Step 3, put the precursor solution prepared in step 2 into a spinneret with an inner diameter of 1.2mm, the receiving device is grounded and rotated directly as a 100mm aluminum roller, the receiving distance is 20cm, the spinning voltage is 20kV...

Embodiment 3

[0045] Embodiment 3: a kind of preparation method of antibacterial interior wall nano-emulsion paint,

[0046] Step 1, solution A: Dissolve 10 parts of tetrabutyl titanate in a mixed solution of 7.5 parts of absolute ethanol and 6.5 parts of acetic acid, and fully stir for 12 hours;

[0047] Solution B: Dissolve 4 parts of acetylacetone and 7.5 parts of absolute ethanol and mix with 6 parts of anhydrous acetic acid under stirring conditions, add 4.44 parts of mineral oil and 0.5 parts of silver nitrate, mix well, and fully stir for 12 hours;

[0048] Step 2, mix A solution and B solution according to the ratio of 1:1, and fully stir for 12 hours to obtain a precursor colloid solution for preparing silver / titanium dioxide nanotubes;

[0049] Step 3, put the precursor solution prepared in step 2 into a spinneret with an inner diameter of 1.1mm, the receiving device is grounded and rotated directly as a 100mm aluminum roller, the receiving distance is 19cm, the spinning voltage i...

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Abstract

The invention belongs to the field of paint and particularly discloses a preparation method of antibacterial nano latex paint for interior walls. Firstly, a precursor colloidal solution of a silver / titanium dioxide nanotube is prepared; a precursor product obtained through spinning is immediately cooled after electrostatic spinning, then put into a muffle furnace and sintered at a constant temperature, and the silver / titanium dioxide nanotube is obtained; the silver / titanium dioxide nanotube is dispersed in water under the condition of stirring, and propylene glycol, a coalescing agent, a wetting agent, a preservative, hydroxyethyl cellulose and a dispersing agent are added and stirred in a grinder to be mixed uniformly; titanium dioxide, triple superphosphate, kaolin and talc powder are added and sufficiently ground in a high-speed grinder, and an acrylic emulsion, a defoaming agent and a thickening agent are added; finally, the mixture is stirred to be uniformly mixed in the grinder, filtered and packaged in barrels, and a finished product of the antibacterial nano latex paint for the interior walls is obtained. The antibacterial nano latex paint for the interior walls is aimed to solve the problem of breeding of bacteria on interior walls of a room and mildewing of the interior walls due to humid weather lasting for a long time.

Description

technical field [0001] The invention relates to the field of coatings, in particular to a preparation method of antibacterial interior wall nano-emulsion paint. Background technique [0002] Driven by the construction industry, China's coatings industry is growing from strength to strength. Statistics show that in 2011, the total output of China's architectural coatings was about 3.5182 million tons, an increase of more than 30% year-on-year. It can be seen that although China's architectural coatings industry has experienced the impact of the global financial crisis in 2008 and the pressure brought by rising raw material prices, its development momentum remains unabated, and it still maintains a relatively high growth rate. [0003] Interior wall paint is an essential material for home decoration. At present, with the enhancement of people's awareness of environmental protection, the requirements for interior wall latex paint for decoration are getting higher and higher, a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D133/00C09D5/14C09D5/02C09D7/61C09D7/63C09D7/65
CPCC08K2003/0806C08K2201/011C08L2205/025C08L2205/035C09D5/025C09D5/14C09D133/04D01F9/10C08L75/04C08K13/04C08K3/08C08K7/24
Inventor 田亮亮李璐刘碧桃闫兴武陈贤程江杨鑫
Owner 上海流丹新型材料科技有限公司
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