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A kind of preparation method of polyester fiber with catalytic degradation function

A polyester fiber, catalytic degradation technology, applied in chemical instruments and methods, separation methods, fiber treatment and other directions, can solve the problem of low durability of catalyst catalytic performance, and achieve stable and durable catalytic degradation performance, high catalytic activity, and simple preparation process. Effect

Active Publication Date: 2019-02-22
旷达纤维科技有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The problem is that the fastness of the catalyst on the fiber and the persistence of the catalytic performance are low

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • A kind of preparation method of polyester fiber with catalytic degradation function
  • A kind of preparation method of polyester fiber with catalytic degradation function
  • A kind of preparation method of polyester fiber with catalytic degradation function

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] The preparation method of polyester fiber with purification function includes the following two parts:

[0034] 1)TiO 2 Preparation of intercalated graphene oxide particles:

[0035] Take 10g 800 mesh expanded graphite and 250g 98% sulfuric acid (H 2 SO 4 ), placed in a 5000mL container. In an ice-water bath, under the condition of 800 revolutions per minute, mechanically stir, make it fully mixed, and then slowly add 20 g of potassium permanganate to complete the reaction. The solution was moved to an oil bath at 40°C and operated at 600 rpm for 60 minutes. Add 300mL deionized water, react at 95℃ for 25min; continue to add 600mL deionized water, stir evenly, add 30g 30% hydrogen peroxide (H 2 O 2 ) Aqueous solution, the solution gradually changes from brown-black to bright yellow. Add deionized water, centrifuge and disperse at 5000 rpm, and wash to neutrality to obtain graphene oxide. Take the above-prepared graphene oxide in a hydrothermal reactor, seal it under 140℃ a...

Embodiment 2

[0040] The preparation method of polyester fiber with purification function includes the following two parts:

[0041] 1)TiO 2 Preparation of intercalated graphene oxide particles:

[0042] Take 8g 2000 mesh expanded graphite and 95g 98% sulfuric acid (H 2 SO 4 ), placed in a 5000mL container. Under the condition of 1000 revolutions per minute in an ice-water bath, mechanically stir, make it fully mixed, and slowly add 15 g of potassium permanganate to complete the reaction. The solution was transferred to an oil bath at 60°C and operated for 100 minutes at 1000 revolutions per minute. Add 500mL deionized water, react at 100℃ for 30min; continue to add 800mL deionized water, stir evenly, add 25g 30% hydrogen peroxide (H 2 O 2 ) Aqueous solution, the solution gradually changes from brown-black to bright yellow. Add deionized water, centrifuge and disperse at 8000 rpm, and wash to neutrality to obtain graphene oxide. Take the above-prepared graphene oxide in a hydrothermal reactio...

Embodiment 3

[0047] The graphene oxide and TiO obtained in Example 1-2 2 Intercalated graphene oxide particles, containing TiO 2 The polyester fibers intercalated with graphene oxide particles were identified, and the results are shown in the accompanying drawings.

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Abstract

The invention discloses polyester fibers with a catalytic degradation function and a preparation method thereof. The method comprises the following steps: firstly preparing TiO2 intercalated graphene oxide particles; cutting functional particles into micro-nano powder with a strong ultraviolet lamp; keeping the powder suspending in a cavity through air flow, and horizontally feeding colored polyester filaments into the cavity; softening the polyester fibers by controlling the temperature in the cavity so as to effectively bond with the powder; and carrying out hot pressing on the polyester filaments bonded with the functional powder to firmly bond the powder and the polyester fibers. The prepared novel polyester fibers have excellent catalytic degradation performance for aldehydes, benzene and other organic matters in vehicles; and the method is simple and feasible, and the catalytic degradation performance of the fibers can be durable and stable.

Description

Technical field [0001] The invention relates to the field of functional fiber materials, in particular to a preparation method of polyester fiber with catalytic degradation function. Background technique [0002] With the continuous growth of automobile consumption, the demand for automotive textile fabrics has also increased steadily. Among them, in addition to the comfort, beauty, economy and durability required by traditional textiles, textile materials for automotive interiors have higher requirements in terms of anti-fouling, flame-retardant, anti-static, anti-ultraviolet and other safety and environmental protection. [0003] At present, people pay more attention to the environment in the car. The national standard GB / T27630-2011 for the concentration of organic matter in the air in the car is implemented. The mandatory standard for the concentration of organic matter in the air in the passenger car will soon be implemented. The specific requirements are as follows: [0004] ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06M11/74D06M11/46B01D53/86B01D53/72D06M101/32
CPCB01D53/8668D06M11/46D06M11/74D06M2101/32
Inventor 吴双全龚旭东姚理荣丁志荣李雅任煜
Owner 旷达纤维科技有限公司
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