Patents
Literature
Hiro is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Hiro

30results about How to "No granulation required" patented technology

Method for preparing semi-aromatic nylon

The invention discloses a method for preparing semi-aromatic nylon and belongs to the technical field of macromolecular material synthesis. The method comprises the following steps: (1) uniformly mixing aliphatic diamine and water of which the weight is two to ten times that of the aliphatic diamine, heating the mixture to the temperature of between 50 and 90 DEG C, adding aromatic diacid into the mixture with stirring till a pH value of the solution reaches 7.0-7.7, continuously stirring for 1 to 5 hours, cooling the solution to room temperature, continuously stirring the solution for 1 to 5 hours again, and filtering and drying to obtain nylon salt for later use; and (2) adding the prepared nylon salt and a solvent to a polymerization kettle in a certain mixture ratio (0.5 to 3.0 g/mL), raising the temperature to between 190 and 230 DEG C under the protection of inert gas, keeping the pressure in the kettle between 2.0 and 3.0 MPa, discharging gas after 1 to 5 hours to make the pressure in the kettle reduced to normal pressure within 1 to 5 hours, raising the temperature to between 210 and 270 DEG C, and continuing to react for 1 to 5 hours, and discharging to obtain a powdery semi-aromatic nylon product. The method has mild reaction condition and low energy consumption; the product is easy to mold and machine; and the method solves the difficult problem of difficult discharging of the semi-aromatic nylon, and is applicable to industrialized production.
Owner:青岛智库生物技术有限公司

Pulverized coal ash and PVC (Poly Vinyl Chloride) composited micro-foaming building template reinforced by long glass fibers, and preparation method of building template

The invention relates to a pulverized coal ash and PVC (Poly Vinyl Chloride) composited micro-foaming building template reinforced by long glass fibers. The building template comprises a PVC composited modified material matrix, and the matrix consists of PVC, a heat stabilizer, a foaming agent, a foam stabilizer, a flexibilizer, an internal lubricant, an external lubricant, pulverized coal ash and high-strength long glass fibers. According to the pulverized coal ash and PVC (Poly Vinyl Chloride) composited micro-foaming building template reinforced by long glass fibers as well as a preparation method of the building template, the pulverized coal ash and the long glass fibers are adopted for filling and reinforcement, so that both the dimensional stability and the economical efficiency of the building template are enhanced greatly; the pulverized coal ash as a recyclable raw material is environment-friendly and energy-saving and can be used for replacing inorganic fillers such as calcium carbonate, so that the economic cost is lowered; in addition, the building template has advantages of light weight, resistance to medium acid-alkali corrosion, recyclability, heat insulation, good mechanical performance, flame retardation, wear resistance and the like; besides, the micro-foaming building template, which is manufactured by virtue of specific auxiliaries and an advanced micro-foaming technology, is environment-friendly, nontoxic, light in weight and resistant to medium acid-alkali corrosion; the service cycle of the building template is prolonged by 4-5 times than that of a wooden template and a bamboo-glue template, and the physical and mechanical properties of the building template are enhanced by 3-4 times; in addition, the building template can be demolded easily, and simultaneously the building template is recyclable, green and environment-friendly and saves the economic cost.
Owner:DAYING COUNTY SIPAIKE NEW MATERIALS

Method of producing three-in-one electrode of solid oxide fuel battery

The invention relates to a preparation method of membrane electrode assembly of solid oxide fuel cell, belonging to the plasma spraying method in the surface engineering area for the preparation of the core parts of the solid oxide fuel cell. The invention aims at preparing a compact electrolyte layer with smaller film thickness and evenly distributed material composition, effectively improving the electrolyte conductivity, reducing the internal resistance of SOFC, increasing the output power, and preparing porous and evenly distributed electrodes. The invention comprises following steps: preparation, spraying a support electrode, spraying an electrolyte layer, spraying cathode or anode. The invention has the advantages that fine nanometer or ultrafine powder can be directly used to spray without granulating; the material change between the function layers shows continuous gradually-changing gradient distribution, which can reduce the interface resistance and avoid the interface stratification; one time continuous forming is integrated with sintering process, and times of sintering are not needed, so that the invention is particularly suitable for spraying SOFC electrodes in the forms of flat plate, tuber, Mono-Block Layer Built and corrugating, large-area nanostructure coating, and short process making of nanometer devices.
Owner:HUAZHONG UNIV OF SCI & TECH

Long-carbon-chain semi-aromatic nylon PA14T and preparation method thereof

The invention relates to a long-carbon-chain semi-aromatic nylon PA14T and a preparation method thereof, belonging to the field of high polymer material synthetic technologies. The repeat unit is shown in the specification, and the degree of polymerization of the long-carbon-chain semi-aromatic nylon PA14T is n which is equal to 2 to 200. The preparation method comprises the following steps: (1) preparing nylon PA14T salt: adding 1,4-terephthalic acid and 1,14-tetradecanedioic diamine into water to perform salt forming reaction; (2) preparing semi-aromatic nylon PA14T: adding the nylon PA14T salt obtained in step (1) and a solvent into a polymerizer, heating up a reaction still to be at 200-240 DEG C under a condition of shielding gas, reacting for 1-4 hours under the pressure of 1.2 to 3 MPa, deflating until normal pressure is achieved and vacuumizing, and then carrying out polymerization reaction to obtain the semi-aromatic nylon PA14T. The PA14T is excellent in performance and is easy to process and form, and has the good market prospect, especially in electronic and electrical, automotive industries and the like; and besides, the long-carbon-chain semi-aromatic nylon PA14T is simple in technology, moderate in reaction condition, short in reaction time and low in energy consumption.
Owner:HENAN JUNHENG IND GRP BIOTECH CO LTD

Novel ignition powder and preparation method thereof

The invention discloses novel ignition powder and a preparation method thereof. The novel ignition powder comprises, by mass percentage, 3-9% of coating agent, 50-70% of main oxidant, 0-15% of auxiliary oxidant, 15-25% of fuel and 1-4% of combustion catalyst. The ignition powder prepared by the method has the advantages that the problems that existing ignition powder is narrow in application range, low in energy, poor in safety performance and complex in preparation process are solved; the prepared ignition powder is good in safety performance, high in energy, good in thermal stability and wide in combustion speed regulation range; meanwhile, the novel ignition powder is less prone to moisture absorption, safe and environmentally friendly, and the whole production, assembling and use process of the ignition powder is free of dust hazards.
Owner:HUBEI INST OF AEROSPACE CHEMOTECH

Manufacturing method of beaded polytrifluorochloroethylene resins

The invention relates to a manufacturing method of beaded polytrifluorochloroethylene resins, which comprises the following steps of: taking trifluorochlor oethylene, high-purity water, an organic dispersant and an initiator under the condition that the mass ratio of the trifluorochlor oethylene, the high-purity water, the organic dispersant and the initiator is 100:(500-1000): (50-200): (0.1-1); placing the high-purity water, the organic dispersant and the initiator in a reaction kettle, and at a stirring speed of 400-500 rmp, feeding the trifluorochlor oethylene into the reaction kettle; carrying out reaction on the obtained mixture for 4-6 hours under the conditions of 0.2-1 Mpa and 20-30 DEG C; and then continuing to react for 2-4 hours at a temperature of 50 DEG C and at a stirring speed of 100-200 rmp; and carrying out washing and drying on the obtained product so as to obtain a beaded polytrifluorochloroethylene resin with a diameter of 0.5-5 mm. The method disclosed by the invention is stable in polymerization rate and narrow in molecular weight distribution, no dust flying occurs in the process of production, and no further granulation treatment is required; the obtained polytrifluorochloroethylene resin is excellent in performances, and can be prepared into tubes, bars and profiles with more complicated shapes through melt injection molding; and no yellowing phenomenon occurs, therefore, the method has good social, economic and environmental benefits.
Owner:山东森福新材料有限公司

Polymer microsphere modifying and flooding agent for high-temperature and high-salinity oil reservoir as well as preparation method and application thereof

The invention discloses a polymer microsphere modifying and flooding agent for a high-temperature and high-salinity oil reservoir as well as a preparation method and application of the polymer microsphere modifying and flooding agent. The modifying and flooding agent is prepared from an oil-soluble emulsifier, an oil-soluble unsaturated diene monomer, an acrylamide monomer, an aromatic ring-containing olefin monomer, a water-soluble emulsifier, an oil-soluble initiator, a cross-linking agent, water and an oily solvent through water-in-oil-in-water double emulsion polymerization. The polymer microsphere profile modifying and flooding agent prepared by the invention is not easy to degrade in a medium with high mineralization degree, molecules of the modifying and flooding agent do not contain groups easy to hydrolyze, so that the rigidity of a polymer molecular chain is increased, the tackifying, salt resistance and temperature resistance of a polymer are improved, and meanwhile, the polymer microsphere modifying and flooding agent is relatively high in breakthrough pressure gradient, relatively strong in expansibility and relatively good in plugging performance; the preparation process is simple, and drying and granulation processes after the conventional polymer microsphere modifying and flooding agent is prepared are omitted.
Owner:成都新驱势石油技术开发有限公司

Method for preparing semi-aromatic nylon

The invention discloses a method for preparing semi-aromatic nylon and belongs to the technical field of macromolecular material synthesis. The method comprises the following steps: (1) uniformly mixing aliphatic diamine and water of which the weight is two to ten times that of the aliphatic diamine, heating the mixture to the temperature of between 50 and 90 DEG C, adding aromatic diacid into the mixture with stirring till a pH value of the solution reaches 7.0-7.7, continuously stirring for 1 to 5 hours, cooling the solution to room temperature, continuously stirring the solution for 1 to 5hours again, and filtering and drying to obtain nylon salt for later use; and (2) adding the prepared nylon salt and a solvent to a polymerization kettle in a certain mixture ratio (0.5 to 3.0 g / mL),raising the temperature to between 190 and 230 DEG C under the protection of inert gas, keeping the pressure in the kettle between 2.0 and 3.0 MPa, discharging gas after 1 to 5 hours to make the pressure in the kettle reduced to normal pressure within 1 to 5 hours, raising the temperature to between 210 and 270 DEG C, and continuing to react for 1 to 5 hours, and discharging to obtain a powdery semi-aromatic nylon product. The method has mild reaction condition and low energy consumption; the product is easy to mold and machine; and the method solves the difficult problem of difficult discharging of the semi-aromatic nylon, and is applicable to industrialized production.
Owner:青岛智库生物技术有限公司

Method of producing three-in-one electrode of solid oxide fuel battery

The invention relates to a preparation method of membrane electrode assembly of solid oxide fuel cell, belonging to the plasma spraying method in the surface engineering area for the preparation of the core parts of the solid oxide fuel cell. The invention aims at preparing a compact electrolyte layer with smaller film thickness and evenly distributed material composition, effectively improving the electrolyte conductivity, reducing the internal resistance of SOFC, increasing the output power, and preparing porous and evenly distributed electrodes. The invention comprises following steps: preparation, spraying a support electrode, spraying an electrolyte layer, spraying cathode or anode. The invention has the advantages that fine nanometer or ultrafine powder can be directly used to spraywithout granulating; the material change between the function layers shows continuous gradually-changing gradient distribution, which can reduce the interface resistance and avoid the interface stratification; one time continuous forming is integrated with sintering process, and times of sintering are not needed, so that the invention is particularly suitable for spraying SOFC electrodes in the forms of flat plate, tuber, Mono-Block Layer Built and corrugating, large-area nanostructure coating, and short process making of nanometer devices.
Owner:HUAZHONG UNIV OF SCI & TECH

Abrasion-resistant LED heat dissipation lamp holder and preparation method thereof

InactiveCN109401284AGood heat dissipationImprove mechanical strength and wear resistanceBrominePolypropylene
The invention relates to the technical field of LED lamp production, and discloses an abrasion-resistant LED heat dissipation lamp holder and a preparation method thereof. The abrasion-resistant LED heat dissipation lamp holder is prepared from the following raw materials in parts by weight: 60-90 parts of polyamide resin, 40-60 parts of polypropylene resin, 5-9 parts of a toughening agent, 15-20parts of an asbestos fiber, 3-6 parts of high alumina bauxite, 0.4-0.7 part of an antioxidant, 0.3-0.8 part of a lubricant, and 0.2-0.5 part of a dispersant. The LED lamp holder has good heat dissipation, abrasion resistance, flame retardancy, safety and environmental protection; polyamide resin and polypropylene resin which are heat conducting materials are taken as main raw materials; the asbestos fiber and the high alumina bauxite are added; on the premise of ensuring good heat dissipation, the mechanical strength and abrasion resistance of the LED lamp holder can be effectively improved; meanwhile, the use of toxic and harmful raw materials containing bromine and heavy metals is reduced; and compared with traditional aluminum lamp holders and ceramic lamp holders, the LED lamp holder prepared by direct injection molding of mixed powder has simple process and low costs.
Owner:河南恒翔塑业科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products