Optical film and method for producing optical film
A manufacturing method and optical film technology, which is applied in the field of optical films, can solve the problems of increased haze of optical films, and achieve the effects of low haze, excellent crack resistance and adhesion
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[0198] The "aqueous solvent" used for preparation of the said optical function layer coating liquid means the solvent which consists of water in 50 mass % or more of components. Of course, 100% by mass pure water not containing other solvents may be used, but in consideration of the dispersion stability of vanadium dioxide-containing microparticles, it is preferable that the content of other organic solvents is small. The solvent constituting the water-based solvent and components other than water are not particularly limited as long as they are compatible with water. Alcohol-based solvents can be preferably used, and isopropanol having a boiling point relatively close to water is preferable among them.
[0199] The wet coating method used in the formation of the above-mentioned optical function layer is not particularly limited, for example, roll coating method, bar coating method, air knife coating method, spray coating method, slide type curtain coating method, or U.S. Paten...
Embodiment
[0350] Hereinafter, although an Example is given and this invention is demonstrated concretely, this invention is not limited to these Examples. In addition, in an Example, the expression "part" or "%" is used, and unless otherwise indicated, it means "part by mass" or "% by mass".
[0351] "Optical film production"
[0352] [Production of Optical Film 101]
[0353] (Preparation of fine particle dispersion liquid 1 containing vanadium dioxide: with particle drying process)
[0354] Ammonium vanadate (NH 4 VO 3 , Wako Pure Chemical Industries, Ltd., special grade) 0.433g, and then slowly drop hydrazine hydrate (N 2 h 4 ·H 2 (0, Wako Pure Chemical Industries, Ltd., special grade) 5% by mass aqueous solution, and a solution 1 having a pH of 9.2 at 23° C. and 55% RH was prepared. The prepared solution 1 was charged into a commercially available autoclave for hydrothermal reaction treatment (Hu-25 type manufactured by Sanai Scientific Co., Ltd., with a Teflon (registered tra...
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