A carbon nanotube composite hydrogel-based phase change material and its preparation method and application
A carbon nanotube composite and phase change material technology, which is applied in the field of carbon nanotube composite hydrogel-based phase change materials and their preparation, can solve the problems of poor thermal conductivity, low use efficiency, short service life and the like, and achieves service life. Long, fast cold storage, good thermal conductivity
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Embodiment 1
[0031] A carbon nanotube composite hydrogel-based phase change material, in parts by weight, said material comprising 1 part of a carbon nanotube composite hydrogel base material, 90 parts of a phase change main energy storage agent, and 1 part of a nucleating agent; Wherein the carbon nanotube composite hydrogel substrate includes 0.2 mg of carbon nanotubes, surfactant, 0.1 g of monomer, 3 mg of initiator and crosslinking agent.
[0032] The surfactant comprises 50 mg of sodium dodecylbenzenesulfonate and 25 mg of dodecyldimethylbenzyl ammonium bromide.
[0033] The monomer is N-isopropylacrylamide, and the crosslinking agent is N,N'-methylenebisacrylamide.
[0034] The initiator is a redox system composed of 100 μL of ammonium persulfate with a mass fraction of 4% and 10 μL of tetramethylethylenediamine.
[0035] The phase change main energy storage agent is a sodium chloride solution with a mass concentration of 15%.
[0036] The nucleating agent is barium fluoride.
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Embodiment 2
[0049] A carbon nanotube composite hydrogel-based phase change material, in parts by weight, said material comprising 5 parts of a carbon nanotube composite hydrogel base material, 98 parts of a phase change main energy storage agent, and 3 parts of a nucleating agent; Wherein the carbon nanotube composite hydrogel substrate includes 2 mg of carbon nanotubes, a surfactant, 0.2 g of a monomer, and 3 mg of an initiator and a crosslinking agent.
[0050] The surfactant comprises 56 mg of sodium dodecylbenzenesulfonate and 28 mg of dodecyldimethylbenzyl ammonium bromide.
[0051] The monomer is N-isopropylacrylamide, and the crosslinking agent is N,N'-methylenebisacrylamide.
[0052] The initiator is a redox system composed of 100 μL of ammonium persulfate with a mass fraction of 4% and 10 μL of tetramethylethylenediamine.
[0053] The phase change main energy storage agent is a potassium chloride solution with a mass concentration of 5%.
[0054] The nucleating agent is barium ...
Embodiment 3
[0067] A carbon nanotube composite hydrogel-based phase change material, in parts by weight, said material comprising 10 parts of a carbon nanotube composite hydrogel base material, 88 parts of a phase change main energy storage agent, and 5 parts of a nucleating agent; Wherein the carbon nanotube composite hydrogel substrate includes 3.5 mg of carbon nanotubes, a surfactant, 0.1 g of a monomer, 4 mg of an initiator and a crosslinking agent.
[0068] The surfactant comprises 50 mg of sodium dodecylbenzenesulfonate and 25 mg of dodecyldimethylbenzyl ammonium bromide.
[0069] The monomer is N-isopropylacrylamide, and the crosslinking agent is N,N'-methylenebisacrylamide.
[0070] The initiator is a redox system composed of 130 μL of ammonium persulfate with a mass fraction of 4% and 13 μL of tetramethylethylenediamine.
[0071] The phase change main energy storage agent is obtained by mixing 10% ammonium chloride and 5% sodium chloride solution at a ratio of 7:2.
[0072] The...
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