Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Method for preparing pesticide from eupatorine

A technology for preparing pesticides and zeilin bases, which is applied in the fields of pesticides, botanical equipment and methods, and chemicals for biological control, etc. Excellent effect, simple preparation process, excellent insecticidal effect

Inactive Publication Date: 2017-07-11
嵊州市派特普科技开发有限公司
View PDF6 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

This product has significant killing and preventive effects on vegetables, fruit trees, flowers, forest trees and field crops of Homoptera, Spleen Acarina and other pests, but the effective insecticide formula of this insecticide is mainly euprine , the insecticidal effect and scope may be slightly worse. In the preparation, the various raw materials are simply mixed to make an insecticide, and there is still room for improvement in the preparation process

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Adopt the method for preparing insecticide from euprine, the preparation steps are as follows:

[0023] 1) Preparation of Eupatorium: take fresh Eupatorium adenophorum, wash, dry and pulverize, soak in extractant at 45-80°C for 1-10 hours, filter, rotary steam, extract, and chromatograph. Concentrated teetherine extract;

[0024] 2) Preparation of the extract: wash and pulverize the mother-of-pearl and lantana, put them into solvent and co-solvent respectively, soak them, filter, rotary steam, and extract to obtain the extract of the plant and the extract of the lantana;

[0025] 3) Combination: Mix the extract of plane grass, bamboo leek, lantana extract and Eupatorium evenly and heat, add surfactant, stir, add stabilizer, water, synergistic leveling agent, mix evenly, let stand , to obtain an insecticide; the present invention fully extracts the effective insecticidal components in Eupatorium adenophorum, planegrass, and lantana, and obtains an insecticide with excel...

Embodiment 2

[0034] Adopt the method for preparing insecticide from euprine, preferred preparation steps are as follows:

[0035] 1) Preparation of Eupatorium: Take the whole plant of Eupatorium adenophorum, wash it with running water, dry it at 45°C, crush it to a 150-mesh sieve, soak it in a mixture of 75% ethanol and ethyl acetate, 75% ethanol and acetic acid The preferred mass ratio of ethyl ester is 5:3, the immersion temperature is preferably 60°C, the time is preferably 3h, filtration, rotary evaporation, the vacuum degree of rotary evaporation is 0.8, the temperature is 50°C, extraction is carried out, and the luster is analyzed by thin layer chromatography. Separation and purification of Eupatorium adenophorum, and the content of Eupatorin A adenophorum A was tested by ultraviolet spectrometry, and then the Eupatorium adenophorum extract was concentrated to liquid extract;

[0036] 2) Preparation of the extract: Take the whole plants of the plane grass, mother of pearl, and lantan...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention provides a method for preparing a pesticide from eupatorine. The method comprises the following steps: 1, preparing eupatorine: taking fresh Eupatorium adenophora Spreng., washing the Eupatorium adenophora Spreng., drying and crushing the Eupatorium adenophora Spreng., immersing the Eupatorium adenophora Spreng. in an extractant at 45-80 DEG C for 1-10 h, filtering the obtained solution, carrying out rotary evaporation, carrying out extraction, carrying out chromatography, and carrying out concentration to obtain eupatorine extract; 2, preparing extract liquids: taking Fragrant Eupatorium Herb, pearl shells and Lantana camara L, washing and crushing above three raw materials, respectively immersing the three raw materials in a solvent and a cosolvent, filtering obtained solutions, carrying out rotary evaporation, and carrying out extraction to obtain a Fragrant Eupatorium Herb extract liquid and a Lantana camara L extract liquid; and 3, mixing: uniformly mixing and heating the Fragrant Eupatorium Herb extract liquid, bamboo juice, the Lantana camara L and eupatorine, adding a surfactant, stirring the obtained mixed solution and the surfactant, adding a stabilizer, water and a synergistic leveling agent, uniformly mixing above substances, and standing the obtained solution to obtain the pesticide. Effective insecticidal components in the Eupatorium adenophora Spreng., the Fragrant Eupatorium Herb and the Lantana camellia L are fully extracted, and the pesticide with the advantages of excellent insecticidal effect, good stability and no pollution to environment is obtained through optimizing pesticide preparation steps.

Description

technical field [0001] The invention belongs to the technical field of pesticides, and in particular relates to a method for preparing pesticides by using euprine. Background technique [0002] Eupatorium adenophorum (scientific name: Eupatorium adenophora Spreng.): Perennial herb or semi-shrub-like plant, with strong and well-developed rhizomes, erect, plant height 30-200 cm, opposite branches, oblique, purple stems, covered with white or rust-colored pubescence, opposite leaves, The leaves are thin, ovate, triangular or diamond-shaped ovate, green on the ventral surface, light-colored on the back, with sparse, thick and irregular serrations on the edge, and wavy shallow serrations or nearly entire margins at the bottom of the inflorescence. The flower head is small and the diameter Up to 6 mm, arranged in corymbs or compound corymbs at branch ends, containing about 40-50 small flowers, tubular flowers bisexual, white. Seed achenes, dark brown. Each plant can produce ab...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): A01N65/44A01N63/02A01N25/30A01P7/04A01P1/00
CPCA01N25/30A01N63/10A01N65/00A01N65/44A01N2300/00Y02A50/30
Inventor 施春华张美芬
Owner 嵊州市派特普科技开发有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products