Method for preparing pesticide from eupatorine
A technology for preparing pesticides and zeilin bases, which is applied in the fields of pesticides, botanical equipment and methods, and chemicals for biological control, etc. Excellent effect, simple preparation process, excellent insecticidal effect
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Embodiment 1
[0022] Adopt the method for preparing insecticide from euprine, the preparation steps are as follows:
[0023] 1) Preparation of Eupatorium: take fresh Eupatorium adenophorum, wash, dry and pulverize, soak in extractant at 45-80°C for 1-10 hours, filter, rotary steam, extract, and chromatograph. Concentrated teetherine extract;
[0024] 2) Preparation of the extract: wash and pulverize the mother-of-pearl and lantana, put them into solvent and co-solvent respectively, soak them, filter, rotary steam, and extract to obtain the extract of the plant and the extract of the lantana;
[0025] 3) Combination: Mix the extract of plane grass, bamboo leek, lantana extract and Eupatorium evenly and heat, add surfactant, stir, add stabilizer, water, synergistic leveling agent, mix evenly, let stand , to obtain an insecticide; the present invention fully extracts the effective insecticidal components in Eupatorium adenophorum, planegrass, and lantana, and obtains an insecticide with excel...
Embodiment 2
[0034] Adopt the method for preparing insecticide from euprine, preferred preparation steps are as follows:
[0035] 1) Preparation of Eupatorium: Take the whole plant of Eupatorium adenophorum, wash it with running water, dry it at 45°C, crush it to a 150-mesh sieve, soak it in a mixture of 75% ethanol and ethyl acetate, 75% ethanol and acetic acid The preferred mass ratio of ethyl ester is 5:3, the immersion temperature is preferably 60°C, the time is preferably 3h, filtration, rotary evaporation, the vacuum degree of rotary evaporation is 0.8, the temperature is 50°C, extraction is carried out, and the luster is analyzed by thin layer chromatography. Separation and purification of Eupatorium adenophorum, and the content of Eupatorin A adenophorum A was tested by ultraviolet spectrometry, and then the Eupatorium adenophorum extract was concentrated to liquid extract;
[0036] 2) Preparation of the extract: Take the whole plants of the plane grass, mother of pearl, and lantan...
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