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Green body molding method of ceramic microbeads

A technology of ceramic microbeads and molding methods, which is applied in the field of special ceramics, can solve the problems of low production efficiency, high production cost, and difficulty in forming small and micro-sized products, and achieve the effects of improving production efficiency, reducing self-wear, and increasing volume density

Active Publication Date: 2020-07-31
中国国检测试控股集团淄博有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The object of the present invention is to provide a green body molding method of ceramic microspheres, which solves the problems of high production cost, low production efficiency, and difficulty in forming small and micro-sized products in the production process of high-quality ceramic microspheres, and has the advantages of simple molding method , high production efficiency, good product performance, and great practical promotion value

Method used

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  • Green body molding method of ceramic microbeads
  • Green body molding method of ceramic microbeads

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Take 20Kg of alumina ceramic microbead green body (92% content) with a particle size of 3mm rolled into shape, heat the liquid silica gel to 120°C and keep the temperature stable, then pour the 20Kg microbead green body Put it into liquid silica gel, and turn on the stirring device at the same time. After 10 minutes, take out the ball blank coated with organic matter with a tool. After 5 minutes, it can be dried and solidified; Secondary pressure molding, the molding pressure is 90MPa, and qualified semi-finished products can be obtained. After low-temperature firing to remove organic matter and high-temperature firing, the product manufacturing is completed.

[0023] After testing, the performance index of the product obtained in this embodiment is as follows: the bulk density is 3.76g / cm 3 , the flexural strength is 500MPa, self-wear ≤0.15g / Kg.h.

Embodiment 2

[0025] Take 10Kg of spray-molded zirconia ceramic microbead body with a particle size of 0.2mm, heat the liquid silica gel to 260°C and keep the temperature stable, then pour 10Kg of the microbead body into the liquid silica gel, and open the Stirring device, after 10 minutes, take out the ball blank coated with organic matter with a tool, and after 5 minutes, it can be dried and solidified; the processed ball blank is subjected to secondary pressure molding through a cold isostatic press, and the shape The pressure is 150MPa, and qualified semi-finished products can be obtained, and the product is manufactured after low-temperature firing to remove organic matter and high-temperature firing.

[0026] After testing, the performance index of the product obtained in this embodiment is as follows: the bulk density is 6.75g / cm 3 , the flexural strength is 1500MPa, self-wear ≤ 6ppm / Kg.h.

Embodiment 3

[0028] Take 5Kg of injection-molded silicon oxide ceramic microbead body with a particle size of 0.3mm, heat the liquid silica gel to 260°C and keep the temperature stable, then pour 5Kg of the microbead body into the liquid silica gel, and open the Stirring device, after 10 minutes, take out the ball blank coated with organic matter with a tool, and after 5 minutes, it can be dried and solidified; the processed ball blank is subjected to secondary pressure molding through a cold isostatic press, and the shape The pressure is 170MPa, and qualified semi-finished products can be obtained, and the product manufacturing is completed after low-temperature firing to remove organic matter and high-temperature firing.

[0029] After testing, the performance index of the product obtained in this embodiment is as follows: the bulk density is 3.26g / cm 3 , the bending strength is 1000MPa, and the hardness (HV) is 1800MPa.

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Abstract

The invention relates to a blank forming method of ceramic microbeads, and belongs to the technical field of special ceramic. The blank forming method comprises the following steps: ceramic powder is preformed to obtain microbead blanks; and then, the microbead blanks are dipped in organic solvent for wrapping, are put in a cylinder of a cold isostatic press for isostatic forming, and are burnt at low temperature and sintered at high temperature to obtain ceramic microbead products. The blank forming method solves the problems of high production cost, low production efficiency and difficult formation of microproducts in the production process of high-quality ceramic microbeads, and has the characteristics of simple forming method, high production efficiency, good product performances and high actual popularization value; the micron-scale ceramic microbead blanks prepared by the forming method can improve the production efficiency by 40%, and can reach the compressive strength of 55-150 MPa; and after high-temperature sintering by different modes and temperatures, the bulk density of the products can be improved by above 5%, and the self-wear consumption is reduced by above 30%.

Description

technical field [0001] The invention relates to a green body forming method of ceramic microbeads, which belongs to the technical field of special ceramics. Background technique [0002] In the past 20 years, isostatic pressing technology has been widely used in ceramic manufacturing, tool manufacturing, plastics, high-voltage electromagnetic porcelain bottles, high-performance materials, military industry and other fields. In the special industrial ceramics industry, cold isostatic pressing technology has gained Large-scale promotion and application. Cold isostatic pressing technology is to use flexible materials such as rubber, plastic or resin as the mold material at room temperature, and use liquid as the pressure transmission medium. It is mainly used for the molding of powder materials and is used for further sintering or hot isostatic pressing. Provide blanks. The body forming method of ceramic microbeads utilizes cold isostatic pressing forming technology, thereby ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B28B3/00C04B35/10C04B35/14C04B35/48C04B35/565C04B35/584
CPCB28B3/003C04B35/10C04B35/14C04B35/48C04B35/481C04B35/565C04B35/584C04B2235/602C04B2235/61
Inventor 张大军李勇陈学江吴萍侯伟华
Owner 中国国检测试控股集团淄博有限公司