Process for the preparation of polyethylene compositions
A technology of ethylene polymers and polymers, applied in the field of gel content of polyethylene, can solve problems such as unsatisfactory production, influence of homogenization of final polymer composition, uneven final polymer composition, etc.
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Embodiment 1
[0266] Example 1: Polyethylene (a) (=ssPE(a)) prepared in the presence of a single-site catalyst of a polymer composition according to the invention, referred to as SSPE1 in the table below
[0267] Catalyst Example: Preparation of Catalyst
[0268] 130 g of the metallocene complex bis(1-methyl-3-n-butylcyclopentadienyl) zirconium(IV) dichloride (CAS No. 151840-68-5) and 9.67 kg of commercially available methyl aluminum A 30% solution of oxane (MAO) in toluene was combined and 3.18 kg of dry purified toluene was added. The complex solution thus obtained was added to 17 kg of silica support Sylopol 55SJ (supplied by Grace) within 2 hours by means of a very slow uniform spray. Keep the temperature below 30°C. The mixture was reacted for 3 hours after complex addition at 30°C.
[0269] Aggregation of SSPE1:
[0270] Pre-polymerization: operating at a temperature of 60 °C and a pressure of 65 bar with 50 dm 3 volume of the loop reactor. 2.5 kg / h of ethylene, 30 kg / h of propa...
Embodiment 2
[0275] Example 2: ssPE(2), hereinafter referred to as SSPE2
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Abstract
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