Electromagnetic shielding paper and preparation method thereof
A technology of electromagnetic shielding and preparation steps, applied in the field of electromagnetic shielding paper and its preparation, can solve the problems of electromagnetic wave leakage, uncontrolled behavior, permanent damage, etc., and achieve the effect of improving stability and stable properties
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Embodiment 1
[0032] An electromagnetic shielding paper and a preparation method thereof, the steps of preparing the electromagnetic shielding paper are as follows:
[0033]Add 2kg of whisker-like carbon nanotubes into 10L of potassium nitrate solution with a mass concentration of 14%, ultrasonically disperse for 1 hour to form a uniform suspension, then add 0.14L of concentrated sulfuric acid with a mass concentration of 95%, and Treat for 8.5 hours to acidify the surface of carbon nanotubes with -COOH functional groups, then rinse with distilled water until neutral and remove salt, and then evaporate and dry at room temperature and low pressure (0.05MPa) for 16 hours to obtain carbon nanotubes with high surface activity; Add the obtained carbon nanotubes and 7kg epoxy resin into 15kg solvent, ultrasonically disperse for 2 hours, then heat up to 160°C, react for 10 hours, and oscillate evenly at the same time. After the reaction is completed, a composite material of carbon nanotubes and the...
Embodiment 2
[0036] An electromagnetic shielding paper and a preparation method thereof, the steps of preparing the electromagnetic shielding paper are as follows:
[0037] Add 1kg of whisker-like carbon nanotubes into 6L of sodium nitrate solution with a mass concentration of 15%, ultrasonically disperse for 1.5h to form a uniform suspension, then add 0.08L of concentrated sulfuric acid with a mass concentration of 98%. Under treatment for 8 hours to acidify the surface of carbon nanotubes with -COOH functional groups, then rinse with distilled water until neutral and remove salt, and then evaporate and dry at normal temperature and low pressure (0.05MPa) for 18 hours to obtain carbon nanotubes with high surface activity; Add the obtained carbon nanotubes and 3kg of furfuryl alcohol resin into 8kg of solvent, ultrasonically disperse for 2.5 hours, then heat up to 170°C, react for 8 hours, and vibrate evenly at the same time. After the reaction is completed, a composite material of carbon n...
Embodiment 3
[0040] An electromagnetic shielding paper and a preparation method thereof, the steps of preparing the electromagnetic shielding paper are as follows:
[0041] Add 1.7kg of whisker-like carbon nanotubes into 10L of 13% sodium nitrate solution, ultrasonically disperse for 1.5h to form a uniform suspension, then add 0.14L of concentrated sulfuric acid with a mass concentration of 98%. Treat at room temperature for 8 hours to acidify the surface of carbon nanotubes with -COOH functional groups, then rinse with distilled water until neutral and remove salt, and then evaporate and dry at room temperature and low pressure (0.05MPa) for 18 hours to obtain carbon nanotubes with high surface activity; Add the obtained carbon nanotubes and 5.5kg of maleimide resin to 15kg of solvent, ultrasonically disperse for 2.5 hours, then heat up to 155°C, react for 9 hours, and shake evenly at the same time. After the reaction is completed, carbon nanotubes and thermosetting resins are obtained. R...
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