Sample clamping device in underground engineering wastewater treatment integrated equipment
A wastewater treatment and integrated equipment technology, applied in the direction of contaminated groundwater/leachate treatment, water/sewage treatment, water/sludge/sewage treatment, etc., can solve the troublesome manual operation process, hidden safety hazards, and impact on underground engineering wastewater Dealing with issues such as integrated equipment productivity
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[0064] The preparation method of described slide bar 8-5-8 comprises the following steps:
[0065] Step 1: Add purified water and 2-acrylamido-2-methylpropylsulfonic acid / acrylamide / acrylic acid terpolymer into the non-foaming stirred reactor, start the stirrer in the non-foaming stirred reactor, Set the rotation speed at 55rpm-101rpm, start the oil tank heater in the bubble-free stirred reactor, raise the temperature to 70.4°C-71.1°C, add alkyl (phenol) polyoxyethylene ether sulfosuccinic acid monoester disodium salt and stir Uniform, react for 47.3 to 58.8 minutes, add lithium bis(trifluoromethanesulfonyl)imide, and the flow rate is 46.401m 3 / min~87.449m 3 Oxygen per min for 0.55 to 0.120 hours; then add 2-[(4-amino-3-bromo-9,10-dihydro-9,10-dioxo-1-anthracenyl) into a bubble-free stirred reactor Amino]-5-methylbenzenesulfonic acid monosodium salt, restart the oil tank heater in the non-bubble stirring reactor, raise the temperature to 87.9℃~120.2℃, keep it warm for 47.9~...
Embodiment 1
[0072] Make the slide bar 8-5-7 of the present invention according to the following steps, and in parts by weight:
[0073] Step 1: Add 262.4 parts of purified water and 54.3 parts of 2-acrylamido-2-methylpropylsulfonic acid / acrylamide / acrylic acid terpolymer into the non-foaming stirred reactor to start the non-foaming stirred reactor The stirrer in the middle, set the rotating speed as 55rpm, start the oil tank heater in the bubble-free stirring reactor, make the temperature rise to 70.4°C, add 57.9 parts of alkyl (phenol) polyoxyethylene ether sulfosuccinic acid monoester disodium salt Stir evenly, react for 47.3 minutes, add 53.9 parts of lithium bis(trifluoromethanesulfonyl)imide, and the flow rate is 46.401m 3 / min of oxygen for 0.55 hours; then add 2-[(4-amino-3-bromo-9,10-dihydro-9,10-dioxo-1-anthracenyl)amino] in a bubble-free stirred reactor - 56.0 parts of monosodium salt of 5-methylbenzenesulfonic acid, start the oil tank heater in the non-bubble stirring reactor ...
Embodiment 2
[0080] Make the slide bar 8-5-7 of the present invention according to the following steps, and in parts by weight:
[0081] Step 1: In the non-foaming stirred reactor, add 487.1 parts of purified water and 96.8 parts of 2-acrylamido-2-methylpropylsulfonic acid / acrylamide / acrylic acid terpolymer to start the non-foaming stirred reactor In the mixer, the set speed is 101rpm, start the oil tank heater in the bubble-free stirring reactor, make the temperature rise to 71.1 ° C, add 166.2 parts of alkyl (phenol) polyoxyethylene ether sulfosuccinic acid monoester disodium salt Stir evenly, react for 58.8 minutes, add 70.0 parts of lithium bis(trifluoromethanesulfonyl)imide, and the flow rate is 87.449m 3 / min of oxygen for 0.120 hours; then add 2-[(4-amino-3-bromo-9,10-dihydro-9,10-dioxo-1-anthracenyl)amino] in a bubble-free stirred reactor - 113.6 parts of 5-methylbenzenesulfonic acid monosodium salt, start the oil tank heater in the non-bubble stirred reactor again, raise the temp...
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