A kind of preparation method of modified carbon fiber thermal insulation composite material
A composite material and modified carbon technology, which is applied in the direction of carbon fiber, fiber treatment, fiber chemical characteristics, etc., can solve the problems of low adsorption performance and poor interfacial bonding between materials, and achieve large specific surface area, high-efficiency heat insulation capacity, high The effect of mechanical strength
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[0020] A method for preparing a modified carbon fiber thermal insulation composite material, comprising the following steps:
[0021] (1) Crush the silicon powder through a 180-mesh sieve, and soak it in hot water at 60°C for 20 minutes. When putting in the hot water, add half of the silicon powder first, then add the remaining silicon powder in 3 times, and then pour off the hot water. Add the activated silica powder into 20% sodium hydroxide solution, stir continuously after being completely submerged and heat to 90°C, and react at this temperature for 8 hours to obtain alkaline silica sol;
[0022] (2) Put the spinning solution in the electrospinning apparatus, wrap the receiver with aluminum foil, and collect the as-spun fibers on the aluminum foil. The process parameters of the spinning process are positive pressure 15kV, negative pressure 1.5kV, and advance rate 0.04 mm / min, the receiving rate is 30r / min, the distance between the needle and the receiver is 15cm, and the ...
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