Pore-forming agent removal method for battery separator and preparation process for lithium-ion secondary battery separator
A preparation process and secondary battery technology, applied in separators/films/diaphragms/spacers, battery components, circuits, etc., can solve problems such as extraction difficulties of thick substrates, shorten extraction time, and solve extraction difficulties , The effect of speeding up the extraction rate
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Embodiment 1
[0028] A method for removing a pore-forming agent for a battery diaphragm, which is applied in the preparation process of a lithium-ion secondary battery diaphragm, and the steps of the method include:
[0029] The diaphragm substrate is pretreated by equipment, and at least a part of the pore-forming agent in the diaphragm substrate is removed in advance; in this embodiment, the pore-forming agent is white oil, but it is not limited thereto; when white oil is at 40°C, the kinematic viscosity 45-55mm 2 / s;
[0030] The pretreated separator substrate is extracted by ultrasonic extraction to extract the pore-forming agent, and ensure that the residual rate of the pore-forming agent in the final battery separator is less than 1%.
[0031] During the ultrasonic extraction process, the ultrasonic frequency is 17KHz, and the ultrasonic extraction time is 10min.
[0032] The equipment includes scraping roller set equipment with at least one pair of scraping roller sets 1 and vacuum...
Embodiment 2
[0046] This embodiment is basically the same as Embodiment 1, except that in the ultrasonic extraction process, the ultrasonic frequency is 28KHz, and the ultrasonic extraction time is 10 minutes.
Embodiment 3
[0048] This embodiment is basically the same as Embodiment 1, except that in the ultrasonic extraction process, the ultrasonic frequency is 17KHz, and the ultrasonic extraction time is 15 minutes.
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Abstract
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