A kind of flexible biomass selenium extraction material and preparation method thereof
A biomass material and biomass technology, applied in chemical instruments and methods, other chemical processes, alkali metal compounds, etc., can solve the problems of serious pollution, selenium selectivity, complex process, high surface reactivity, etc., and achieve favorable adsorption Function, large surface roughness, avoiding the effect that is not easy to recycle
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Embodiment 1
[0028] (1) Prepare a NaOH solution with a concentration of 5 wt%, and add 8 g of sisal per 100 mL of NaOH solution, cut the sisal into pieces and add it to the NaOH solution. In an environment of 60 °C, after stirring for 4 h, it was taken out and cooled to room temperature, washed with distilled water until neutral, and dried to obtain a biomass cellulose precursor.
[0029] (2) Prepare NaClO with a concentration of 5 wt% 2 solution, and adjust the pH to 4 with glacial acetic acid to obtain NaClO 2 Mixture. Per 100 mL NaClO 2 Add 5 g of biomass cellulose precursor to the mixed solution, and add the biomass cellulose precursor to NaClO 2 The mixture was stirred in the environment of 60 °C for 4 h, then taken out and cooled to room temperature, washed with distilled water until neutral, and dried to obtain biomass cellulose.
[0030] (3) Add 10 g of biomass cellulose to 100 mL of deionized water, stir mechanically to form a paste-like slurry, and after ultrasonic treatment,...
Embodiment 2
[0035] (1) Prepare a NaOH solution with a concentration of 1 wt%. Add 2 g of jute per 100 mL of NaOH solution, cut jute into pieces and add it to the NaOH solution. In an environment of 60 °C, after stirring for 1 h, take it out and cool it to room temperature, wash it with distilled water until it is neutral, and dry it to obtain a biomass cellulose precursor.
[0036] (2) Prepare NaClO with a concentration of 1 wt% 2 solution, and adjust the pH to 2 with glacial acetic acid to obtain NaClO 2 Mixture. Per 100 mL NaClO 2Add 2 g of biomass fiber precursor to the mixed solution, and add the biomass fiber precursor to NaClO 2 The mixture was stirred in the environment of 60 °C for 1 h, then taken out and cooled to room temperature, washed with distilled water until neutral, and dried to obtain biomass cellulose.
[0037] (3) Add 5 g of biomass cellulose to 100 mL of deionized water, stir mechanically to form a paste slurry, and after ultrasonic treatment, apply the paste slur...
Embodiment 3
[0042] (1) A KOH solution with a concentration of 10 wt% was prepared, and 8 g of green hemp was added to every 100 mL of KOH solution, and the green hemp was chopped and added to the KOH solution. In an environment of 100 °C, after stirring for 4 h, it was taken out and cooled to room temperature, washed with distilled water until neutral, and dried to obtain a biomass cellulose precursor.
[0043] (2) Prepare NaClO with a concentration of 10 wt% 2 solution, and adjust the pH to 6 with glacial acetic acid to obtain NaClO 2 Mixture. Per 100 mL NaClO 2 Add 20 g of biomass fiber precursor to the mixed solution, and add the biomass fiber precursor to NaClO 2 The mixed solution was stirred for 4 h in an environment of 100 °C, then taken out and cooled to room temperature, washed with distilled water until neutral, and dried to obtain biomass cellulose.
[0044] (3) Add 25 g of biomass cellulose to 100 mL of deionized water, stir mechanically to form a paste-like slurry, and af...
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