A Method for Guiding Micro-Nanomotors Using Magnetically Responsive Topological Orbitals
A micro-nano, motor technology, applied in the direction of nanotechnology, nanotechnology, nanotechnology, etc. for sensing, can solve the problems of microbial death, difficulty in applying biomedical fields, poor biocompatibility of ferromagnetic materials, etc., and achieve simplification The effect of the preparation process
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Embodiment 1
[0032] Fe used to form topological orbitals 3 o 4 @PVP nanoparticles, prepared according to the literature (Adv Mater 2014, 26(7), 1058-1064) using a solvothermal method, have superparamagnetism and monodispersity. The tubular micro-nanomotor prepared according to the literature was placed under a scanning electron microscope (SEM, S-4800, Hitachi Co., Ltd., Japan) for microscopic characterization.
[0033] SEM pictures of micro-nano motors taken by scanning electron microscope (SEM, S-4800, Hitachi Co., Ltd., Japan) figure 1 shown.
Embodiment 2
[0035] Orientation process of micro-nano motors:
[0036] Sodium cholate solution (this solution is a surfactant, similar effects can also be achieved with other surfactants), H 2 o 2 solution, Fe 3 o 4 @PVP nanoparticle suspension and tubular micro-nano motor suspension are mixed, and ultrasonic vibration is used to disperse them evenly. The H 2 o 2 Solution concentration is 7vt%, sodium cholate aqueous solution concentration is 0.5wt%, Fe 3 o 4 @PVP nanoparticles concentration is 94mg / mL.
[0037] Take an appropriate amount of the above liquid and drop it on the glass slide, and use a magnet to apply a directional magnetic field.
[0038] Utilize an inverted fluorescent microscope (LeicaDMI 3000M) to photograph the motion state of the micro-nano motor in Example 2, and intercept the motor motion timing diagram and schematic diagram as shown in figure 2 shown. It can be observed that when the topological orbit is not formed, the micro-nanomotor makes a circular motio...
Embodiment 3
[0040] Using a directional magnetic field to control the micro-nano motor to move along a predetermined trajectory experiment:
[0041] Sodium cholate solution, H 2 o 2 solution, Fe 3 o 4 @PVP nanoparticle suspension and tubular micro-nano motor suspension are mixed, and ultrasonic vibration is used to disperse them evenly. The H 2 o 2 Solution concentration is 6vt%, sodium cholate aqueous solution concentration is 0.4wt%, Fe 3 o 4 @PVP nanoparticles concentration is 75mg / mL.
[0042] Take an appropriate amount of the above-mentioned liquid and drop it on the glass slide, apply a directional magnetic field with a magnet, and change the direction of the magnetic field.
[0043] Utilize an inverted fluorescent microscope (LeicaDMI 3000M) to take pictures of the motion state of the micro-nano motor in Example 3, and intercept the timing diagram and motion trajectory diagram as image 3 shown. Under the action of a directional magnetic field, Fe 3 o 4 @PVP nanoparticle...
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