Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Copolymer and its application and oil-based drilling fluid stabilizer and its preparation method and oil-based drilling fluid

A technology of oil-based drilling fluid and copolymer, which is applied in the field of oil-based drilling fluid, can solve the problems of poor stability of oil-based drilling fluid, etc., and achieve the effects of cleaning the wellbore, improving the stability of the settlement, and improving the stability of the emulsion

Active Publication Date: 2020-05-22
CHINA UNIV OF PETROLEUM (EAST CHINA)
View PDF6 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of the present invention is to overcome the problem of poor stability of oil-based drilling fluid in the prior art under high temperature conditions, to provide a copolymer and its application, oil-based drilling fluid stabilizer and its preparation method and oil-based drilling fluid liquid

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Copolymer and its application and oil-based drilling fluid stabilizer and its preparation method and oil-based drilling fluid
  • Copolymer and its application and oil-based drilling fluid stabilizer and its preparation method and oil-based drilling fluid
  • Copolymer and its application and oil-based drilling fluid stabilizer and its preparation method and oil-based drilling fluid

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0026] The fourth aspect of the present invention provides a kind of preparation method of oil-based drilling fluid stabilizer, wherein, the preparation method comprises:

[0027] (1) fatty acid and fatty acid polymer are mixed and dissolved;

[0028] (2) performing the first reaction at 150-200° C. after mixing the mixture obtained in step (1) with the polyamine compound;

[0029] (3) Cool the reaction product obtained in step (2) to 20-35°C and mix it with diacid and / or dianhydride, and then carry out the second reaction at 150-200°C;

[0030] And optionally, after cooling the reaction product of the second reaction to 50-70° C., it is mixed with unsaturated fatty acid for dilution.

[0031] In the present invention, preferably, the molar ratio of fatty acid, fatty acid polymer, polyamine compound, diacid and / or dianhydride is 1:1-3:0.1-0.5::0.03-0.1, preferably 1:2 -2.5: 0.2-0.4: 0.03-0.05.

[0032] In the present invention, in order to further improve the performance ef...

Embodiment 1

[0044] (1) Mix oleic acid and dimerized fatty acid (purchased from Shanghai Zhipu Chemical Co., Ltd., trade mark is DMA-1080) to fully dissolve the dimerized fatty acid;

[0045](2) Mix the mixture obtained in step (1) with tetraethylenepentamine, react for 6 hours under the condition of an oil bath at 170°C, and remove the moisture generated by the reaction during the reaction;

[0046] (3) After the above reaction is completed, cool the system to 20°C, add adipic acid, raise the temperature to 170°C at a rate of 10°C / min, and react for 4 hours.

[0047] (4) After the reaction is finished, the reaction product is cooled to 60° C., and the same volume of oleic acid as the product is added for dilution.

[0048] Among them, the molar ratio of oleic acid, dimer fatty acid, tetraethylenepentamine and adipic acid is 1:2.5:0.3:0.05. Stabilizer A1 was obtained.

Embodiment 2

[0050] (1) Mix linolenic acid and dimerized fatty acid (purchased from Shanghai Zhipu Chemical Co., Ltd., brand name is DMA-1080) to fully dissolve the dimerized fatty acid;

[0051] (2) Mix the mixture obtained in step (1) with triethylenediamine, and react for 8 hours under the condition of an oil bath at 150° C., and remove the moisture generated by the reaction during the reaction;

[0052] (3) After the above reaction is completed, cool the system to 30°C, add maleic anhydride, raise the temperature to 150°C at a rate of 15°C / min, and react for 3 hours.

[0053] (4) After the reaction is finished, the reaction product is cooled to 60° C., and the same volume of oleic acid as the product is added for dilution.

[0054] Among them, the molar ratio of oleic acid, dimer fatty acid, triethylenediamine and maleic anhydride is 1:2:0.2:0.03. Stabilizer A2 is obtained.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention relates to the technical field of oilfield chemistry, and discloses a copolymer and application thereof, an oil-based drilling fluid stabilizer and a preparation method thereof, and an oil-based drilling fluid, and the copolymer comprises a structural unit provided by a fatty acid, a structural unit provided by a fatty acid polymer, a structural unit provided by a polyamine compound,and a structural unit provided by a diacid and / or an acid anhydride. The oil-based drilling fluid stabilizer containing the copolymer is added to the oil-based drilling fluid to improve the emulsionstability and sedimentation stability of the oil-based drilling fluid, and has good high temperature resistance, and the purpose of safe drilling can be achieved.

Description

technical field [0001] The invention relates to the technical field of oilfield chemistry, in particular to a copolymer and its application, an oil-based drilling fluid stabilizer, a preparation method thereof, and an oil-based drilling fluid. Background technique [0002] With the development of oil and gas exploration and development towards deeper and more complex formations, more and more difficulties are faced in the drilling process. Oil-based drilling fluid has been widely used in deep wells, ultra-deep wells, horizontal wells, extended-reach wells and complex formation conditions due to its superior performance in temperature resistance, inhibition, lubrication, and protection of oil and gas layers compared with water-based drilling fluids. Oil-based drilling fluid is a kind of drilling fluid based on water-in-oil emulsion. The main components are: oil phase (diesel oil, mineral oil, etc.), brine, emulsifier, fluid loss control agent, organic soil, and weighting mate...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): C08G69/34C09K8/035C09K8/32
CPCC08G69/34C09K8/035C09K8/32
Inventor 黄贤斌孙金声吕开河刘敬平
Owner CHINA UNIV OF PETROLEUM (EAST CHINA)
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products