Copolymer and its application and oil-based drilling fluid stabilizer and its preparation method and oil-based drilling fluid
A technology of oil-based drilling fluid and copolymer, which is applied in the field of oil-based drilling fluid, can solve the problems of poor stability of oil-based drilling fluid, etc., and achieve the effects of cleaning the wellbore, improving the stability of the settlement, and improving the stability of the emulsion
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[0026] The fourth aspect of the present invention provides a kind of preparation method of oil-based drilling fluid stabilizer, wherein, the preparation method comprises:
[0027] (1) fatty acid and fatty acid polymer are mixed and dissolved;
[0028] (2) performing the first reaction at 150-200° C. after mixing the mixture obtained in step (1) with the polyamine compound;
[0029] (3) Cool the reaction product obtained in step (2) to 20-35°C and mix it with diacid and / or dianhydride, and then carry out the second reaction at 150-200°C;
[0030] And optionally, after cooling the reaction product of the second reaction to 50-70° C., it is mixed with unsaturated fatty acid for dilution.
[0031] In the present invention, preferably, the molar ratio of fatty acid, fatty acid polymer, polyamine compound, diacid and / or dianhydride is 1:1-3:0.1-0.5::0.03-0.1, preferably 1:2 -2.5: 0.2-0.4: 0.03-0.05.
[0032] In the present invention, in order to further improve the performance ef...
Embodiment 1
[0044] (1) Mix oleic acid and dimerized fatty acid (purchased from Shanghai Zhipu Chemical Co., Ltd., trade mark is DMA-1080) to fully dissolve the dimerized fatty acid;
[0045](2) Mix the mixture obtained in step (1) with tetraethylenepentamine, react for 6 hours under the condition of an oil bath at 170°C, and remove the moisture generated by the reaction during the reaction;
[0046] (3) After the above reaction is completed, cool the system to 20°C, add adipic acid, raise the temperature to 170°C at a rate of 10°C / min, and react for 4 hours.
[0047] (4) After the reaction is finished, the reaction product is cooled to 60° C., and the same volume of oleic acid as the product is added for dilution.
[0048] Among them, the molar ratio of oleic acid, dimer fatty acid, tetraethylenepentamine and adipic acid is 1:2.5:0.3:0.05. Stabilizer A1 was obtained.
Embodiment 2
[0050] (1) Mix linolenic acid and dimerized fatty acid (purchased from Shanghai Zhipu Chemical Co., Ltd., brand name is DMA-1080) to fully dissolve the dimerized fatty acid;
[0051] (2) Mix the mixture obtained in step (1) with triethylenediamine, and react for 8 hours under the condition of an oil bath at 150° C., and remove the moisture generated by the reaction during the reaction;
[0052] (3) After the above reaction is completed, cool the system to 30°C, add maleic anhydride, raise the temperature to 150°C at a rate of 15°C / min, and react for 3 hours.
[0053] (4) After the reaction is finished, the reaction product is cooled to 60° C., and the same volume of oleic acid as the product is added for dilution.
[0054] Among them, the molar ratio of oleic acid, dimer fatty acid, triethylenediamine and maleic anhydride is 1:2:0.2:0.03. Stabilizer A2 is obtained.
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