A kind of color test paper for rapid detection of cyanide and its preparation and detection method
A technology of cyanide and test paper, which is applied in the field of chromogenic test paper for rapid detection of cyanide and its preparation and detection. It can solve the problems of complex and cumbersome operation, high detection cost, and not suitable for large-scale screening of samples, and achieve simple and fast operation process. , improve detection efficiency, low detection cost
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Embodiment 1
[0047] 1.1 Preparation of color test paper and color test paper
[0048] 1) The mass concentration of the preparation is sodium hydroxide 3g / L, isonicotinic acid 15g / L, triton X-100 3g / L, barbituric acid 3g / L, methyl vinyl ether-maleic anhydride copolymer 60g / L mixed solution is used as test paper soaking solution, and the solvent is pure water;
[0049] 2) Pour the prepared test paper soaking solution into a special enamel plate, soak the 3MM filter paper from the test paper soaking solution at a constant speed, take it out, hang it to drain, and send it to a 50°C drying oven to dry for 40-45 minutes;
[0050] 3) Cut the dried 3MM filter paper into strips with a width of 0.6cm, paste the cut 3MM filter paper on a 30×8cm test paper substrate and press it tightly, and cut into 8×0.6cm strips. Obtain the color test paper.
[0051] 1.2 Determination of the detection limit of the color test paper obtained in the above 1.1
[0052] Take a number of negative samples of liquor wi...
Embodiment 2
[0067] 2.1 Preparation of color test paper and color test paper
[0068] 1) The mass concentration of the preparation is sodium hydroxide 8g / L, isonicotinic acid 12g / L, triton X-100 1g / L, barbituric acid 10g / L, methyl vinyl ether-maleic anhydride copolymer 30g / L mixed solution is used as test paper soaking solution, and the solvent is pure water;
[0069] 2) and 3) with embodiment 1.
[0070] The determination of the detection limit, detection accuracy verification, and specificity detection results of the color test paper obtained in the above 2.1 are basically the same as those in Example 1, and will not be repeated here.
Embodiment 3
[0072] 3.1 Preparation of color test paper and color test paper
[0073] 1) The mass concentration of the preparation is sodium hydroxide 12g / L, isonicotinic acid 8g / L, triton X-100 5g / L, barbituric acid 15g / L, methyl vinyl ether-maleic anhydride copolymer 90g / L mixed solution is used as test paper soaking solution, and the solvent is pure water;
[0074] 2) and 3) with embodiment 1.
[0075] The determination of the detection limit of the color test paper obtained in the above 3.1, the detection accuracy verification, and the specificity detection results are basically the same as those in Example 1, and will not be repeated here.
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