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Heat treatment process of ceramic reinforced iron-based composite material

An iron-based composite material and process technology, applied in the field of composite materials, can solve problems such as difficulty in meeting the requirements of wear resistance of materials, and achieve the effect of improving wear resistance

Inactive Publication Date: 2018-10-19
KUNMING UNIV OF SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] With the continuous development of modern industry, the consumption of wear-resistant materials is increasing day by day, and traditional steel materials have been difficult to meet the needs of materials for wear resistance

Method used

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  • Heat treatment process of ceramic reinforced iron-based composite material
  • Heat treatment process of ceramic reinforced iron-based composite material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A heat treatment process for a ceramic reinforced iron-based composite material, the specific steps are as follows:

[0018] (1) Apply an anti-oxidation coating on the surface of the sample to be heat treated, then put it into a box furnace, vacuumize it, and fill it with nitrogen to ensure that the oxygen content is ≦5%, and the pressure in the furnace is stable at 60mbar;

[0019] (2) Heat up to 650°C at a heating rate of 30°C / h, hold for 0.5h, and then heat the sample to 930°C at a heating rate of 60°C / h.

[0020] (3) Insulate at 930°C for 3 hours, take out the sample and cool it in the air until room temperature;

[0021] (4) Tempering: Heat the sample at 20°C to 350°C for 1 hour and then cool in the furnace.

[0022] The structure diagram of the composite material after heat treatment in this embodiment is as follows figure 2 shown. After heat treatment, the carbides in the matrix are refined, the particles are well combined with the matrix, and there is no hea...

Embodiment 2

[0024] A heat treatment process for a ceramic reinforced iron-based composite material, the specific steps are as follows:

[0025] (1) Apply anti-oxidation paint on the surface of the sample to be heat treated, then put it into a box furnace, vacuumize, fill with nitrogen, ensure that the oxygen content is ≦5%, and the pressure in the furnace is stable at 65mbar;

[0026] (2) Heating to 650°C at a heating rate of 35°C / h, keeping the temperature for 1 hour, and then heating the sample to 980°C at a heating rate of 68°C / h.

[0027] (3) Insulate at 980°C for 3 hours, take out the sample and cool it in the air until room temperature;

[0028] (4) Tempering: Heat the sample at 25°C / h to 400°C for 1.5h and then cool in the furnace.

[0029] The performance test results of the composite material in this embodiment are shown in Table 1.

Embodiment 3

[0031] A heat treatment process for a ceramic reinforced iron-based composite material, the specific steps are as follows:

[0032] (1) Apply anti-oxidation paint on the surface of the sample to be heat treated, then put it into a box furnace, vacuumize it, fill it with nitrogen, ensure that the oxygen content is ≦5%, and the pressure in the furnace is stable at 70mbar;

[0033] (2) Heat up to 650°C at a heating rate of 45°C / h, hold for 0.8h, and then heat the sample to 1000°C at a heating rate of 75°C / h.

[0034] (3) Insulate at 1000°C for 5 hours, take out the sample and cool it in the air until room temperature;

[0035] (4) Tempering: Heat the sample at 30°C / h to 400°C for 1.8h and then cool in the furnace.

[0036] The performance test results of the composite material heat treated in this embodiment are shown in Table 1.

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Abstract

The invention discloses a heat treatment process of a ceramic reinforced iron-based composite material. The process comprises the following steps: (1) coating an antioxidant coating on a surface of asample to be heat-treated, placing the sample in a box furnace, vacuuming, charging nitrogen, ensuring the oxygen content is less than or equal to 5% and the furnace pressure is between 60 to 70 mbar;(2) heating the sample to 650 DEG C at a heating speed of 30-50 DEG C / h, insulating for 1 hour, and heating the sample to 900-1000 DEG C at a heating rate of 60-80 DEG C / h; wherein when the temperature of the furnace exceeds 1000 DEG C, the heating rate is at 15-20 DEG C / h; (3) carrying out insulation at 930-1080 DEG C for 2-6 hours, and fetching the sample in the air and cooling the sample tillthe temperature is decreased to the room temperature; (4) tempering: heating the sample to 350-450 DEG C at the speed of 20-35 DEG C / h, insulating for 1-2 hours, and cooling in furnace. The heat treatment process improves wear resistance of the composite material, and effectively avoids separation of the ceramic particles from the matrix and the phenomenon of cracking in the composite zone.

Description

technical field [0001] The invention relates to the technical field of composite materials, in particular to a heat treatment process for ceramic reinforced iron-based composite materials. Background technique [0002] With the continuous development of modern industry, the consumption of wear-resistant materials is increasing day by day, and traditional steel materials have been difficult to meet the needs of materials for wear resistance. Ceramic-metal wear-resistant composite materials have both the high hardness and high wear resistance of ceramics and the good toughness of metal, which solves the problem of the contradiction between high hardness and toughness in traditional steel materials. At present, the preparation process of ceramic-metal composite materials at home and abroad The research is getting deeper and deeper, and the heat treatment process is the key link to maximize the potential of composite materials. Due to the great difference in the physical and che...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C21D1/72C21D5/00
CPCC21D1/72C21D5/00
Inventor 张孝足蒋业华冯晶周谟金
Owner KUNMING UNIV OF SCI & TECH