Electrolysis polishing method for preparing pure titanium and titanium alloy EBSD (electron back-scattered diffraction) sample
An electrolytic polishing and titanium alloy technology, applied in the field of metal material processing, can solve the problems of complicated operation and high cost, and achieve the effects of improving sample quality, good light transmittance, and avoiding electrolyte corrosion.
Inactive Publication Date: 2018-11-13
HUANGHUAI UNIV
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The invention relates to the technical field of processing of metal materials, in particular to an electrolysis polishing method for preparing a pure titanium and titanium alloy EBSD (electron back-scattered diffraction) sample. The electrolysis polishing method comprises the following steps of a, selecting a pure titanium or titanium alloy sheet with thickness of 0.5 to 1mm, and respectively grinding both sides of the pure titanium or titanium alloy sheet by 280# and 400# abrasive papers; b, sequentially grinding one surface, ground by the 400# abrasive paper, of the pure titanium or titaniumalloy sheet by 600#, 800#, 1000# and 1200# abrasive papers; c, selecting three to five samples, and grinding and smoothing the burrs of the sample by the 1200# abrasive paper; d, putting the pure titanium or titanium alloy sheet into electrolysis polishing equipment for electrolysis polishing; e, cleaning the pure titanium or titanium alloy sample after electrolysis polishing for the first time;f, cleaning the fetched pure titanium or titanium alloy sample for the second time, fetching out, and blow-drying, so as to obtain the pure titanium and titanium alloy EBSD sample.
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