A kind of apu-al high-frequency high-dielectric low-loss material and preparation method thereof
A high-dielectric, low-loss technology, applied in the field of high-frequency, high-dielectric and low-loss materials and their preparation, can solve problems such as restricting development and increasing losses, and achieve the effects of good applicability, simple process, and excellent mechanical properties
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Embodiment 1
[0040] A preparation method of APU-Al high-frequency high-dielectric low-loss material, comprising the steps of:
[0041] (1) Heat the Al powder at 120°C for 0.5h;
[0042] (2) Weigh 4g of APU precursor and 9g of Al powder, add to a beaker to stir and mix, and ultrasonically disperse with an ultrasonic power of 320W for 1h, so that the aluminum powder is evenly distributed;
[0043] (3) Add 2g of APU curing agent to the homogeneously dispersed precursor in step (2), stir and mix, then ultrasonically disperse again, the ultrasonic power is 320W, and the time is 1h;
[0044] (4) transfer the mixed slurry that step (3) obtains into a high-viscosity spray gun and spray on a polytetrafluoroethylene plate to be a resin film with a thickness of 0.5mm;
[0045] (5) The resin film after step (4) is sprayed, solidifies 48h under room temperature, guarantees the in-situ polymerization reaction of acrylic polyurethane, obtains APU-Al high-frequency high-dielectric low-loss material (such...
Embodiment 2
[0048] A preparation method of APU-Al high-frequency high-dielectric low-loss material, comprising the steps of:
[0049] (1) Heat the Al powder at 120°C for 0.5h;
[0050] (2) Weigh 8g of APU precursor and 18g of Al powder, add to a beaker to stir and mix, and ultrasonically disperse, the ultrasonic power is 320W, and the time is 1h, so that the aluminum powder is evenly distributed;
[0051] (3) Add 4g of APU curing agent to the homogeneously dispersed precursor in step (2), stir and mix, then ultrasonically disperse again, the ultrasonic power is 320W, and the time is 1h;
[0052] (4) transfer the mixed slurry that step (3) obtains into a high-viscosity spray gun and spray on a polytetrafluoroethylene plate to be a resin film with a thickness of 1mm;
[0053] (5) curing the resin film sprayed in step (4) for 48 hours at room temperature to ensure the in-situ polymerization reaction of acrylic polyurethane to obtain an APU-Al high-frequency, high-dielectric and low-loss mater...
Embodiment 3
[0056] A preparation method of APU-Al high-frequency high-dielectric low-loss material, comprising the steps of:
[0057] (1) Heat the Al powder at 120°C for 0.5h;
[0058] (2) Weigh 2g of APU precursor and 7g of Al powder, add to a beaker to stir and mix, and ultrasonically disperse, the ultrasonic power is 320W, and the time is 1h, so that the aluminum powder is evenly distributed;
[0059] (3) Add 1g of APU curing agent to the homogeneously dispersed precursor in step (2), after stirring and mixing, ultrasonically disperse again with an ultrasonic power of 320W and a time of 1h;
[0060] (4) transfer the mixed slurry that step (3) obtains into a high-viscosity spray gun and spray on a polytetrafluoroethylene plate to be a resin film with a thickness of 0.5mm;
[0061] (5) curing the resin film sprayed in step (4) for 48 hours at room temperature to ensure the in-situ polymerization of acrylic polyurethane to obtain APU-Al high-frequency, high-dielectric and low-loss materi...
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