Preparation method of ice blast base oil with natural sour and sweet note

A base oil, sweet and sour technology, applied in the field of tobacco flavors and fragrances, can solve the problems of unstable state of explosive beads, weak aroma of synthetic flavors, affecting the molding of explosive beads, etc., achieving good compatibility, strong aroma, and solving the problem of thin aroma. Effect

Inactive Publication Date: 2019-03-15
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the aroma of synthetic flavors is relatively thin, and its chemical properties are active, so it is easy to react with base oil and wall materials, which leads to an unstable state during the online molding process of popping beads, thus affecting the molding of popping beads

Method used

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  • Preparation method of ice blast base oil with natural sour and sweet note
  • Preparation method of ice blast base oil with natural sour and sweet note

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0014] A kind of preparation method of the quick-fried pearl base oil with natural sour-sweet fragrance that embodiment 1 provides, its specific steps are as follows:

[0015] (1) Take 100g of schisandra chinensis and 100g of jujube seed as raw materials, add tap water accounting for 10 times the weight of the mixed raw materials, soak at room temperature for 12 hours, heat at 60°C under normal pressure for reflux extraction for 4 hours, collect the distillate with a condenser, and separate the oil and water to obtain Volatile oil;

[0016] (2) Dissolve the volatile oil obtained in step (1) into 2000 times of its weight of polyglycerol castor, and add Tween 60 whose weight of the mixture is 0.2‰, filter to remove impurities and insolubles, and collect the filtrate;

[0017] (3) Ultrasonicate the filtrate collected in step (2) for 1 hour at a temperature of 40° C. and a frequency of 30 kHz, and then let it stand for 3 hours after the ultrasonic wave is finished, which is the pe...

Embodiment 2

[0018] A kind of preparation method of the quick-fried pearl base oil with natural sour-sweet fragrance that embodiment 2 provides, its specific steps are as follows:

[0019] (1) Take 200g of schisandra chinensis and 100g of jujube kernels as raw materials, add tap water accounting for 15 times the weight of the mixed raw materials, soak for 8 hours at room temperature, heat to 65°C under normal pressure for reflux extraction for 3 hours, collect the distillate with a condenser, and separate the oil and water get volatile oil;

[0020] (2) Dissolve the volatile oil obtained in step (1) in 5000 times of its weight of polyglycerol ricinoleate, and add Tween 60 whose weight of the mixture is 0.4‰, filter to remove impurities and insolubles, and collect the filtrate;

[0021] (3) Sonicate the filtrate collected in step (2) for 1.5h at a temperature of 30°C and a frequency of 35kHz, and let it stand for 4 hours after the ultrasonication is over, which is the said pearl-popping bas...

Embodiment 3

[0022] A kind of preparation method of the quick-fried pearl base oil with natural sour-sweet fragrance that embodiment 3 provides, its specific steps are as follows:

[0023] (1) Take 150 g of schisandra chinensis and 300 g of jujube seed as raw materials, add tap water accounting for 15 times the weight of the mixed raw materials, soak at room temperature for 12 hours, heat and reflux under normal pressure for extraction for 5 hours, collect distillate with a condenser, and obtain volatile oil after oil-water separation;

[0024] (2) Dissolve the volatile oil obtained in step (1) into 8000 times of its weight of polyglycerol ricinoleate, and add Tween 60 whose weight of the mixture is 0.5‰, filter to remove impurities and insolubles, and collect the filtrate;

[0025] (3) Ultrasonicate the filtrate collected in step (2) for 2 hours at a temperature of 50°C and a frequency of 28kHz, and let it stand for 2 hours after the ultrasonication is completed, which is the pearl-popping...

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Abstract

The invention provides a preparation method of ice blast base oil with natural sour and sweet note. The preparation method of the ice blast base oil comprises the following specific preparation steps:taking raw materials of fructus schisandrae and semen ziziphi spinosae according to the mass ratio of (1 to 2) to (1 to 2) for mixing, adding tap water, soaking at room temperature for 8 to 24 hours,heating, refluxing and extracting at normal pressure for 1 to 5 hours, collecting distillate by using a condenser and carrying out oil and water separation to obtain volatile oil, then adding the volatile oil into polyglycerol polyricinoleate, adding Tween 60, filtering and collecting filtrate, carrying out ultrasonic treatment at 20 to 60 DEG C or below for 0.5 to 2 hours and standing still for2 to 12 hours after the ultrasonic treatment is finished to obtain the ice blast base oil with the natural scour and sweet note. The ice blast base oil disclosed by the invention can bring obvious sour and sweet note, strong aroma, as well as comfortable and nature property; in addition, the ice blast base oil can be well compatible with a wall material, so that the problems of thin aroma and unstable molding caused by the addition of synthetic spices into the ice blast base oil are well solved.

Description

technical field [0001] The invention relates to the field of flavors and fragrances for tobacco, in particular to a preparation method of poppear base oil with natural sweet and sour aroma. Background technique [0002] Popping beads is a special process for flavoring cigarette auxiliary materials and a major innovation in the tobacco industry. The method of popping beads and flavoring improves the safety of cigarette products and greatly enriches the types of flavoring materials. In recent years, major tobacco companies have increased investment in the research and development of puffed pearls, and launched a large number of puffed puffed cigarette products with their own characteristics. important direction. [0003] The essence used in the base oil of the popcorn is basically a synthetic flavor, which plays an important role in enhancing the aroma of the popcorn and enriching the aroma of the smoke. However, the aroma of synthetic flavors is relatively thin, and its che...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02A24B15/30A24B3/12
CPCC11B9/02A24B3/12A24B15/30A24B15/302C11B9/022C11B9/025C11B9/027
Inventor 蹇顺华陈胜孙炜炜苗丽坤彭建
Owner HUBEI CHINA TOBACCO IND
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