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Graphene island fiber and manufacturing method thereof

A technology of sea-island fiber and manufacturing method, applied in the field of graphene sea-island fiber and its manufacturing, to achieve the effects of improving immunity, enhancing far-infrared performance, and stimulating vitality

Active Publication Date: 2019-05-03
SHANGHAI DEFULUN CHEM FIBER
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

So far, there is no report on the use of graphene exclusively for the preparation of polyester sea-island fibers

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0046] S1. Preparation of graphene masterbatch: 60% of 80nm biomass graphene powder prepared by hydrothermal carbonization of biomass resources by weight percentage, 25% of dispersant Pluronic P123 and 15% of Surfactant alcohol ether sulfate is mixed, through stirring, dispersing, obtain graphene slurry; Then use 15% graphene slurry to blend with 65% pure terephthalic acid PTA, 20% ethylene glycol EG to obtain mixed solution, again Add the catalyst sodium aluminate and stir evenly, and then introduce it into the reaction kettle for esterification reaction. The amount of the catalyst added is 1% of the weight of the mixed solution; , final shrinkage, casting, cooling, granulation, and drying to obtain graphene masterbatch.

[0047] S2, preparation of graphene polyester island component: blend 18% graphene masterbatch with dried 82% PET, stir evenly, and melt with screw extruder to prepare graphene polyester island component ;

[0048] S3. Preparation of graphene sea-island pr...

Embodiment 2

[0052] S1. Preparation of graphene masterbatch: 65% of 80nm biomass graphene powder prepared by hydrothermal carbonization of biomass resources by weight percentage, 15% of dispersant Pluronic P123 and 20% of Surfactant alcohol ether sulfate is mixed, through stirring, dispersing, obtain graphene slurry; Then use 18% graphene slurry to blend with 61% pure terephthalic acid PTA, 21% ethylene glycol EG to obtain mixed solution, again Add the catalyst manganese acetate and stir evenly, and then introduce it into the reactor for esterification reaction, the amount of the catalyst added is 0.5% of the weight of the mixed solution; import the esterified mixture into the polycondensation kettle for polycondensation reaction, Final shrinkage, tape casting, cooling, granulation, and drying to obtain graphene masterbatch.

[0053] S2. Preparation of graphene polyester island components: blend 22% graphene masterbatch with dried 78% PET, stir evenly, and melt with screw extruder to prepa...

Embodiment 3

[0057] Embodiment 3 Preparation of graphene sea-island fiber three

[0058] S1. Preparation of graphene masterbatch: 45% of 80nm biomass graphene powder prepared by hydrothermal carbonization of biomass resources by weight percentage, 28% of dispersant Pluronic P123 and 27% of Surfactant alcohol ether sulfate is mixed, through stirring, dispersing, obtain graphene slurry; Then use 15% graphene slurry to blend with 65% pure terephthalic acid PTA, 20% ethylene glycol EG to obtain mixed solution, again Add the catalyst sodium aluminate and stir evenly, and then introduce it into the reaction kettle for esterification reaction. The amount of the catalyst added is 1.8% of the weight of the mixed solution; , final shrinkage, casting, cooling, granulation, and drying to obtain graphene masterbatch.

[0059] S2, preparation of graphene polyester island component: blend 18% graphene masterbatch with dried 82% PET, stir evenly, and melt with screw extruder to prepare graphene polyester...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention relates to a graphene island fiber and a manufacturing method thereof. The manufacturing method comprises the following steps of preparing graphene master batch from a functional graphene material through esterification polymerization, and then blending and melting the graphene master batch and PET to obtain a graphene island composition; melting and blending the graphene island composition and a soluble polyester marine composition to obtain graphene island protofilaments, and conducting working processes of bundling, drafting, tension heat setting, curling, oiling, relaxation heat setting, cutting and the like to obtain the graphene island fiber. The graphene island fiber can reduce the surface resistivity of a material, quickly release generated electrostatic charge, endowthe surface of the material with certain lubricity at the same time and further reduce the friction coefficient so as to inhibit and reduce the generation of electrostatic charge. The biocompatibility is high, and the graphene island fiber is a non-toxic, environment-friendly and efficient functional textile and has the far infrared function, antibacterial function, bacteriostatic function and antistatic function of graphene fibers.

Description

technical field [0001] The invention belongs to the technical field of synthetic fiber production, and in particular relates to a graphene sea-island fiber and a manufacturing method thereof. Background technique [0002] With the development of economy and social life, people's requirements for multifunctional textiles are increasing day by day, especially non-toxic, green, far infrared, antibacterial and antibacterial, antistatic, with unique metallic luster, no chemical dyeing and finishing, natural and lasting color There is a strong demand for textiles with other functions. The sea-island composite fiber fabric feels soft and smooth, and can be made into a fabric with high density, hygroscopicity, water repellency, and unique aesthetics and fashion style; the sea-island composite fiber has a small linear density and a large fiber specific surface area. High coverage, bulkiness, warmth retention and adsorption, which make the fabric have strong dust absorption, decontam...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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IPC IPC(8): D01F8/14D01F1/10D01F1/09C08G63/183C08G63/84
Inventor 李东华陆育明王佳欢冯忠耀朱亚宏杨成周永华杨卫忠李忠赵学东王缘
Owner SHANGHAI DEFULUN CHEM FIBER
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