Graphene island fiber and manufacturing method thereof
A technology of sea-island fiber and manufacturing method, applied in the field of graphene sea-island fiber and its manufacturing, to achieve the effects of improving immunity, enhancing far-infrared performance, and stimulating vitality
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[0045] Example 1
[0046] S1. Preparation of graphene masterbatch: 60% of 80nm biomass graphene powder prepared by the hydrothermal carbonization of biomass resources, 25% of dispersant Pluronic P123 and 15% of Surfactant alcohol ether sulfate is mixed, stirred and dispersed to obtain graphene slurry; then 15% graphene slurry is mixed with 65% purified terephthalic acid PTA, 20% ethylene glycol EG to obtain a mixed solution, and then Add catalyst sodium aluminate, stir evenly, introduce into the reaction kettle to carry out esterification reaction, and the addition amount of the catalyst is 1% of the weight of the mixture; introduce the esterified mixture into the polycondensation kettle to carry out polycondensation reaction, and then undergo pre-condensation , final shrinkage, casting, cooling, granulation and drying to obtain graphene masterbatch.
[0047] S2. Preparation of graphene polyester island components: blend 18% of graphene masterbatch with 82% of dried PET, stir...
Example Embodiment
[0051] Example 2
[0052] S1. Preparation of Graphene Masterbatch: 65% of 80nm biomass graphene powder prepared by the hydrothermal carbonization of biomass resources, 15% of dispersant Pluronic P123 and 20% of Surfactant alcohol ether sulfate is mixed, stirred and dispersed to obtain graphene slurry; then 18% graphene slurry is mixed with 61% purified terephthalic acid PTA, 21% ethylene glycol EG to obtain a mixed solution, and then Add catalyst manganese acetate, stir evenly, introduce into the reaction kettle to carry out esterification reaction, the addition amount of the catalyst is 0.5% of the weight of the mixture; introduce the esterified mixture into the polycondensation kettle to carry out polycondensation reaction, and then undergo pre-shrinking, Final shrinkage, strip casting, cooling, granulation and drying to obtain graphene master batches.
[0053] S2. Preparation of graphene polyester island components: blend 22% of graphene masterbatch with 78% of dried PET, ...
Example Embodiment
[0057] The preparation of embodiment 3 graphene sea-island fiber three
[0058] S1. Preparation of graphene masterbatch: 45% of 80nm biomass graphene powder prepared by the hydrothermal carbonization of biomass resources, 28% of dispersant Pluronic P123 and 27% of Surfactant alcohol ether sulfate is mixed, stirred and dispersed to obtain graphene slurry; then 15% graphene slurry is mixed with 65% purified terephthalic acid PTA, 20% ethylene glycol EG to obtain a mixed solution, and then Add catalyst sodium aluminate, stir evenly, introduce into the reaction kettle to carry out esterification reaction, the addition amount of the catalyst is 1.8% of the weight of the mixture; introduce the esterified mixture into the polycondensation kettle to carry out polycondensation reaction, and then undergo pre-condensation , final shrinkage, casting, cooling, granulation and drying to obtain graphene masterbatch.
[0059] S2. Preparation of graphene polyester island components: blend 18%...
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