Gutta-percha tip composite and DLP printing application thereof
A technology of composite materials and gutta-percha, which is applied in dentistry, dental preparations, dental prostheses, etc., can solve the problems that the precision of finished products needs to be improved, and achieve excellent antibacterial effects, high precision, and increased compatibility.
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Embodiment 1
[0028] A gutta-percha tip composite material based on DLP printing is prepared from the following components in parts by weight of modified nano-barium sulfate, modified nano-silver and photosensitive resin:
[0029] Modified nano barium sulfate: 10 parts,
[0030] Modified nano silver: 10 parts,
[0031] Photosensitive resin: 80 parts;
[0032] The specific steps are: add modified nano-barium sulfate and modified nano-silver to the photosensitive resin in batches according to the proportion, and under the condition of heating (45°C) and avoiding light, stir each time evenly, and stir for 6 hours, and finally obtain a DLP-based gutta-percha tip composites.
[0033] The preparation method of modified nano-barium sulfate and modified nano-silver powder is the same: first dissolve titanate coupling agent UP-801 in an appropriate amount of 40°C absolute ethanol to make the concentration reach 2wt%, and then add an appropriate amount of nano-barium sulfate Or nano-silver, so tha...
Embodiment 2
[0037] A gutta-percha tip composite material based on DLP printing is prepared from the following components in parts by weight of modified nano-barium sulfate, modified nano-silver and photosensitive resin:
[0038] Modified nano zirconia: 15 parts,
[0039] Modified nano silver: 15 parts,
[0040] Photosensitive resin: 70 parts;
[0041] The specific steps are: add modified nano-barium sulfate and modified nano-silver to the photosensitive resin in batches according to the proportion, and under the condition of heating (45°C) and avoiding light, stir each time evenly, and stir for 5 hours to finally obtain a DLP-based gutta-percha tip composites.
[0042] The preparation method of modified nano-zirconia and modified nano-silver powder is the same: first dissolve stearic acid in an appropriate amount of 40°C absolute ethanol to make the concentration reach 1.5wt%, add nano-zirconia or nano-silver, and make it with The mass-to-volume ratio between the surface modifier solut...
Embodiment 3
[0046] A gutta-percha tip composite material based on DLP printing is prepared from the following components in parts by weight of modified nano-barium sulfate, modified nano-silver and photosensitive resin:
[0047] Modified nano barium sulfate: 10 parts,
[0048] Modified nano silver: 20 parts,
[0049] Photosensitive resin: 70 parts;
[0050] The specific steps are: add the obtained modified nano-barium sulfate and modified nano-silver to the photosensitive resin in batches according to the proportion, and under the condition of heating (45°C) and avoiding light, stir evenly each time, stir for 4 hours, and finally get A gutta-percha tip composite based on DLP printing.
[0051] The preparation method of modified nano-barium sulfate and modified nano-silver powder is the same: first dissolve titanate coupling agent UP-801 in an appropriate amount of 40°C absolute ethanol to make the concentration reach 2.5wt%, then add nano-barium sulfate Or nano-silver, so that the mass...
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