Fire assaying analysis method for gold-containing solution
A gold assay analysis and solution technology, which is applied in the field of fire assay gold analysis of gold-containing solutions, can solve the problems of unclean blowing, analysis errors, and inability to form sponge gold, etc., and achieve the effect of accurate analysis
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[0023] A fire assay method for gold-containing solution, the steps comprising:
[0024] ①Sampling: Weigh the sample according to the predicted gold content of the gold-containing solution and put it into the cremation cup;
[0025] ②Evaporation: heat the cremation cup until the sample is semi-dry;
[0026] 3. Adjust pH: wash the semi-dry matter obtained in step 2 with alkaline solution until the remaining solid does not react;
[0027] ④ Heating: in step ③, the obtained solid is mixed with lead powder, and heated in a high-temperature furnace at 1000° C. for 1 hour to obtain molten metal;
[0028] ⑤Shaping: Pour the molten metal obtained in step ④ into the mold while it is still hot, cool it, and knock out the lead button;
[0029] ⑥ Ash blowing: blow the lead button at 1050 ℃ for 1 hour to obtain gold particles and weigh them;
[0030] ⑦ Constant volume: Dissolve the gold particles in aqua regia, determine the volume, measure the impurities in it by ICP method, and invert ...
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