Detection method for Xianling Gubao capsule finished product

Abstract

The invention discloses a detection method for a Xianling Gubao capsule finished product. The Xianling Gubao capsule comprises the following traditional Chinese medicines including herba epimedii, radix dipsaci, radix salviae miltiorrhizae, rhizoma anemarrhenae, fructus psoraleae and radix rehmanniae. The preparation method comprise the following steps that: smashing the radix dipsaci, the radix salviae miltiorrhizae and the fructus psoraleae into fine powder; adding water into the herba epimedii, the rhizoma anemarrhenae and the radix rehmanniae to be decocted for three times; blending decoction liquor, and concentrating to obtain thick paste; adding the fine powder, and evenly mixing to obtain granules; and drying and adding the granules into capsules to obtain the Xianling Gubao capsulefinished product. The detection method comprises the following steps that: authenticating the radix salviae miltiorrhizae and the fructus psoraleae by the same thin layer chromatography, authenticating the herba epimedii and the radix dipsaci by the same thin layer chromatography, and authenticating the rhizoma anemarrhenae. The authentication of two medicines, i.e., the radix dipsaci and the rhizoma anemarrhenae, is added, so that the detection of the contents of the Xianling Gubao capsule establishes clear authentication with high specificity, authentication is more comprehensive, and the quality of the Xianling Gubao capsule finished product can be subjected to scientific, feasible, effective and reliable control. The same thin layer chromatography is adopted to independently authenticate two medicines, so that authentication time is shortened, and cost is lowered.

Description

technical field [0001] The invention belongs to the technical field of quality detection of Xianling Gubao capsules, and in particular relates to a detection method for finished products of Xianling Gubao capsules. Background technique [0002] Xianlinggubao Capsule nourishes the liver and kidneys, promotes blood circulation and clears collaterals, strengthens tendons and bones, and is used for osteoporosis caused by liver and kidney deficiency, blood stasis blocking collaterals. The contents of Bao capsules contain Epimedium, Dipsacus, Salvia, Anemarrhena, Psoralen, and Rehmannia glutinosa. [0003] However, in the original standard of the existing finished product, only the active ingredient tanshinone ⅡA in Danshen, the active ingredient icariin in epimedium, and the active ingredients psoralen and isopsoralen in psoralen were specified as qualitative indicators. TLC identification, less identification of active ingredients, and independent identification, low utilizatio...

AI Technical Summary

Problems solved by technology

[0003] However, in the original standard of the existing finished product, only the active ingredient tanshinone ⅡA in Danshen, the active ingredient icariin in epimedium, and the active ingredients psoralen and isopsoralen in psoralen were specified as qualitative indicators. TLC identification, less identification of active ingredients, and independent identification, low utilization rate of thin-layer plates, few identification items, long identification and detection time, low efficiency and high cost; disclosed in Chinese patent application (authorized announcement number CN100533139C) A detection method for Xianling Gubao pharmaceutical preparations was developed. In Xianling Gubao, only Danshen and Psoraleae were identified separately, but Epimedium, Dipsacus, and Anemarrhena were not identified, and the identification was not comprehensive. Time-consuming identification, unable to fully control the quality of pharmaceutical products

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