Preparation method of test contrast card for rapidly determining residual content of organophosphorus pesticides
A technology of organophosphorus and test cards, which is applied in the direction of material analysis by observing the influence of chemical indicators, and analysis by making materials undergo chemical reactions, can solve the problem of being unable to determine the approximate content of pesticide residues, and meet the professional quality requirements The effect of low cost, good effect and simple preparation method
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Embodiment 1
[0019] Embodiment 1: the preparation method of methimphos test control card, concrete operations are as follows:
[0020] (1) Take the powder of the standard phenimin, add acetonitrile to dissolve and make a 0.104mg / mL solution;
[0021] (2) Preparation of diluent: Take 13.61g of potassium dihydrogen phosphate, add distilled water to dissolve it, and distill it to 500mL to obtain a 0.2mol / L potassium dihydrogen phosphate solution, take 4g of sodium hydroxide, add distilled water to dissolve it And dilute to 500mL with distilled water to get 0.2moL / L sodium hydroxide solution, mix 50mL of 0.2moL / L potassium dihydrogen phosphate solution with 35ml of 0.2moL / L sodium hydroxide solution, dilute with freshly boiled cold water to 200mL, shake well to get a buffer solution with pH 7.2 as a diluent;
[0022] (3) Take the solution in step (1) and dilute it with the diluent in step (2) to a concentration of 0.104×10 -2 mg / mL, 0.208×10 -3 mg / mL, 0.104×10 -3 mg / mL, 0.521×10 -4 mg / mL ...
Embodiment 2
[0025] Embodiment 2: the preparation method of parathion test contrast card, concrete operations are as follows:
[0026] (1) Take parathion standard powder, add acetonitrile to dissolve and make a 0.128mg / mL solution;
[0027] (2) Preparation of diluent: Take 2g of sodium hydroxide, add distilled water to dissolve it, and dilute to 500mL with distilled water to obtain a 0.1mol / L sodium hydroxide solution, take 1.36g of potassium dihydrogen phosphate, add 0.1mol / L hydrogen Sodium oxide 79mL, dilute to 200mL with distilled water to obtain a pH7.4 buffer solution, as a diluent;
[0028] (3) Take the solution in step (1) and dilute it with the diluent in step (2) to a concentration of 0.128×10 -2 mg / mL, 0.256×10 -3 mg / mL, 0.128×10 -3 mg / mL, 0.640×10 -4 mg / mL parathion solution, while the diluent is used as a blank control solution;
[0029] (4) Pipette 50 μL of parathion solution and blank control solution of different concentrations in step (3) and add them dropwise on the ...
Embodiment 3
[0031] Embodiment 3: the preparation method of methyl parathion test contrast card, concrete operation is as follows:
[0032] (1) Take methyl parathion standard powder, add acetonitrile to dissolve and make a 0.120 mg / mL solution;
[0033] (2) Preparation of diluent: Take 5.59g of dipotassium hydrogen phosphate and 0.41g of potassium dihydrogen phosphate, add distilled water to dissolve them, and dilute to 1000mL to obtain a buffer solution with a pH of 8.0 as a diluent;
[0034] (3) Take the solution in step (1) and dilute it with the diluent in step (2) to a concentration of 0.120×10 -2 mg / mL, 0.240×10 -3 mg / mL, 0.150×10 -3 mg / mL, 0.8×10 -4 mg / mL methyl parathion solution, while the diluent is used as a blank control solution;
[0035](4) Pipette 50 μL of different concentrations of methyl parathion solution and blank control solution in step (3) and add them dropwise on the pesticide residue test card. After standing at room temperature for 15 minutes, pinch with your ...
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