A kind of antibacterial textile material and preparation method thereof
A technology for textile materials and raw materials, applied in the field of antibacterial textile materials and their preparation, can solve the problems that the safety cannot be completely guaranteed, reduce the toughness and elasticity of textile materials, etc., and achieve good biocompatibility, good adsorption, and good elasticity. Effect
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Embodiment 1
[0044] The preparation of embodiment 1 silver / shell powder / chitosan microsphere
[0045] S1: Use 3% acetic acid solution as solvent, add 9.3 parts of chitosan to make a 5% chitosan acetic acid solution, make 0.2 parts of silver nitrate into a 0.4mol / L solution, add chitosan In the sugar acetic acid solution, stir at 40°C for 30 minutes, add sodium borohydride solution, shake and react for 3 hours, add 0.5 parts of nano-shell powder, shake evenly, and obtain silver / shell powder / chitosan sol;
[0046] S2: Take 100mL of liquid paraffin as the dispersed phase and 3mL of emulsifier span80 (mass concentration 6%) into the flask in turn, stir evenly under nitrogen protection, add 10mL of the sol prepared in step S1 as the continuous phase into the above mixed solution, Stir until the emulsification is uniform, add 5mL of cross-linking agent glutaraldehyde (mass concentration 4%) to cross-link and solidify chitosan, centrifuge at high speed after 5 hours to break the emulsion, discard...
Embodiment 2
[0047] The preparation of embodiment 2 copper / shell powder / chitosan microsphere
[0048] S1: Use 3% acetic acid solution as solvent, add 9.2 parts of chitosan to make a 5% chitosan acetic acid solution, make 0.3 parts of copper nitrate into a 0.25mol / L solution, add chitosan In the sugar acetic acid solution, using chitosan as a reducing agent, shaking and reacting for 3 hours, adding 0.5 parts of nano-shell powder, shaking evenly, to obtain copper / shell powder / chitosan sol;
[0049] The operation method of S2 is the same as embodiment 1.
Embodiment 3 2
[0050] The preparation of embodiment 3 titanium dioxide / shell powder / chitosan microspheres
[0051] S1: Use 3% acetic acid solution as solvent, add 9.3 parts of chitosan to make a 5% chitosan acetic acid solution, make 0.2 parts of titanium dioxide into a 0.2mol / L solution, add chitosan In the acetic acid solution, shake for 3 hours, add 0.5 parts of nano-shell powder, shake evenly, and obtain titanium dioxide / shell powder / chitosan sol;
[0052] The operation method of S2 is the same as embodiment 1.
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