Nano-phytoncide composition with good stability and preparation method thereof
A technology of phytondine and its composition, which is applied in the field of nano-phytondine composition and its preparation, can solve the problems of reducing stability, reducing practicability, and not being able to play a role stably, achieving strong stability and strong practicability , Remarkable deodorizing effect
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[0024] In one embodiment, the preparation method of the nano-phenadol comprises the following steps:
[0025] (1) Cinnamomum camphora branches and leaves are pulverized;
[0026] (2) Carry out supercritical carbon dioxide extraction with the pulverized Cinnamomum camphora branches and leaves obtained in step (1) in the presence of a carrier agent, collect the extract, concentrate under reduced pressure, and obtain phytondor;
[0027] (3) Dissolving the linoleum oil and the phytondine obtained in the step (2) in ether, and slowly adding a surfactant dissolved in deionized water dropwise while supersonicating, to obtain final product.
[0028] Preferably, the branches and leaves of Cinnamomum camphora in the step (1) are crushed and passed through a sieve with an aperture of 3 to 6 mm; more preferably, the branches and leaves of Cinnamomum camphora in the step (1) are crushed and passed through a sieve with an aperture of 5 mm.
[0029] Preferably, the carrier is selected from ...
Embodiment 1
[0051] Embodiment 1 of the present invention provides a composition of nano-phenadol, which comprises 40 parts of nano-phenadol, 15 parts of plant essential oil, and 60 parts of water in parts by weight.
[0052]The plant essential oils include thyme essential oil, clove essential oil, tea tree essential oil and osmanthus essential oil, the weight ratio of which is 1:2:1:5; the thyme essential oil is purchased from Jishui County Jianmin Natural Perfume Oil Factory; the clove essential oil is purchased from Hubei Jiufenglong Chemical Co., Ltd.; the tea tree essential oil was purchased from Jishui County Weihai Medicinal Oil Factory; the osmanthus essential oil was purchased from Shandong Tengwang Chemical Co., Ltd.
[0053] The preparation method of described nano-phenidol comprises the following steps:
[0054] (1) Cinnamomum camphora branches and leaves are pulverized and passed through a 3mm aperture sieve;
[0055] (2) under the extraction pressure of 14MPa, under the cond...
Embodiment 2
[0063] Embodiment 2 of the present invention provides a composition of nano-phenadol, which comprises 55 parts of nano-phenadol, 25 parts of plant essential oil, and 80 parts of water in parts by weight.
[0064] The plant essential oils include thyme essential oil, clove essential oil, tea tree essential oil and sweet-scented osmanthus oil in a weight ratio of 1:3:3:7; the thyme essential oil is purchased from Jishui County Jianmin Natural Perfume Oil Factory; the clove essential oil is purchased from Hubei Jiufenglong Chemical Co., Ltd.; the tea tree essential oil was purchased from Jishui County Weihai Medicinal Oil Factory; the osmanthus essential oil was purchased from Shandong Tengwang Chemical Co., Ltd.
[0065] The preparation method of described nano-phenidol comprises the following steps:
[0066] (1) Cinnamomum camphora branches and leaves are pulverized and passed through a 6mm aperture sieve;
[0067] (2) under the extraction pressure of 18MPa, under the conditio...
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