Homogenized alumina ceramic and preparation method thereof
A technology of alumina ceramics and alumina ceramic powder, which is applied in the field of homogenized alumina ceramics and its preparation, can solve the problems of inability to obtain homogenized alumina ceramics, etc., and achieves low cost, improved uniformity, and heat export. easy effect
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[0030] As mentioned above, the present invention provides a homogenized alumina ceramic and a preparation method thereof.
[0031] In a first aspect, according to an embodiment of the present invention, a method for preparing a homogenized alumina ceramic is provided, the method comprising the following steps:
[0032] S1, prepare mixed slurry,
[0033] Mix a certain mass ratio of silica sol, water-soluble organic matter and alumina ceramic powder in turn to obtain a mixed slurry;
[0034] S2. Preparation of homogeneous alumina ceramics, including:
[0035] injecting the mixed slurry into a mold and controlling the mold to rapidly suspend in a liquid nitrogen environment to solidify the mixed slurry to obtain a green body;
[0036] The green body is demolded and post-treated to obtain a homogeneous alumina ceramic.
[0037] In the above preparation method, as the liquid phase for preparing the slurry, the silica sol can be an alkaline silica sol or an acidic silica sol, whi...
Embodiment 1
[0062] Step 1: Slurry preparation, mix polyvinylpyrrolidone, silica sol with a concentration of 15wt%, and a pH of 3.6, and alumina ceramic powder in a mass ratio of 1.1:43.9:55, and perform ball milling to obtain alumina ceramic slurry; wherein The alumina ceramic powder contained 10 wt % of particles with an average particle size of 50 nm and 90 wt % of particles with an average particle size of 2 μm, and the ball milling time was 28 h.
[0063] Step 2: Preparation of homogenized alumina ceramics, the above slurry was degassed in a vacuum for 20 minutes and injected into the mold, and it was quickly suspended in liquid nitrogen and fully cured for 0.5 hours, and then demoulded to obtain a green body; the green body was dried at room temperature for 24 hours, 1500 The homogenized alumina ceramic material can be prepared by sintering at ℃ for 2 h.
Embodiment 2
[0065] Step 1: Slurry preparation, mix polyvinylpyrrolidone, silica sol with a concentration of 15 wt %, pH 3.6, and alumina ceramic powder in a mass ratio of 2.5:42.5:55 and perform ball milling to obtain alumina ceramic slurry; wherein The alumina ceramic powder contained 10 wt % of particles with an average particle size of 50 nm and 90 wt % of particles with an average particle size of 2 μm, and the ball milling time was 28 h.
[0066] Step 2: Preparation of homogenized alumina ceramics, the above slurry was degassed in a vacuum for 20 minutes and injected into the mold, and it was quickly suspended in liquid nitrogen and fully cured for 0.5 hours, and then demoulded to obtain a green body; the green body was dried at room temperature for 24 hours, 1500 The homogenized alumina ceramic material can be prepared by sintering at ℃ for 2 h.
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