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Microfiltration membrane and its preparation method and application

A technology of microfiltration membrane and membrane casting liquid, applied in the field of microfiltration membrane and its preparation, can solve the problems of low membrane pure water flux and high energy consumption equipment, and meet the requirements of high selectivity, improved water flux and energy consumption reduced effect

Active Publication Date: 2022-04-08
INST OF BAST FIBER CROPS CHINESE ACADEMY OF AGRI SCI
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the pore size of the charged nanofiltration membrane is small, and a sufficient pressure (above 0.6MPa) is required to be applied during the operation, and the energy consumption and equipment requirements are very high, and the pure water flux of the membrane is small.

Method used

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  • Microfiltration membrane and its preparation method and application
  • Microfiltration membrane and its preparation method and application
  • Microfiltration membrane and its preparation method and application

Examples

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preparation example Construction

[0061] The preparation method of microfiltration membrane of the present invention, comprises the steps:

[0062] S1, dissolving the polyionic liquid in an organic solvent;

[0063] S2, adding a modifying agent to the above solution for dissolution and then ultrasonically dispersing to obtain a casting solution;

[0064] S3, spreading the casting solution on a polytetrafluoroethylene plate and then drying it;

[0065] S4, soaking the polytetrafluoroethylene plate in step S3 in water, taking it out, and peeling it off to obtain a microfiltration membrane.

[0066] The organic solvent suitable for the preparation method of the present invention is not particularly limited, as long as it can dissolve the polyionic liquid. In one embodiment of the present invention, the organic solvent is N,N-dimethylformamide or dimethylsulfoxide.

[0067] In one embodiment of the present invention, the modifier is polyvinylidene fluoride.

[0068] Further, the mass fraction of polyvinylidene...

Embodiment 1

[0072] The preparation method of microfiltration membrane, comprises the steps:

[0073] S1, dissolving the polyionic liquid in N,N-dimethylformamide;

[0074] S2. Add a modifier polyvinylidene fluoride with a mass fraction of 12% to the above solution for blending, and after fully dissolving, ultrasonically remove air bubbles for 10 minutes to obtain a casting solution;

[0075] S3. After spreading the above-mentioned casting solution on the polytetrafluoroethylene board, evaporate in a blast drying oven at 80° C. for 2 hours;

[0076] S4. After immersing the polytetrafluoroethylene plate in water in step S3 to complete the phase inversion process, take it out and peel it off to obtain a microfiltration membrane.

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Abstract

The invention relates to a microfiltration membrane and its preparation method and application. The microfiltration membrane is a polyionic liquid membrane made of polyionic liquid, and the polyionic liquid membrane has a pore size of 0.1 μm-1 μm and a porosity of 75 %‑85%. Compared with the prior art, the present invention has the following beneficial effects: 1) the microfiltration membrane has higher mechanical properties, solvent resistance and ion exchange capacity; 2) the microfiltration membrane is made of polyionic liquid, possessing The electrical properties can separate amino acid mixtures, with high selectivity and strong applicability; 3) The porous and large pore structure of the microfiltration membrane reduces the pressure and energy consumption requirements and improves the water flux.

Description

technical field [0001] The invention relates to the technical field of filtration membrane materials, more specifically, to a microfiltration membrane and a preparation method thereof, a filter medium including the microfiltration membrane, a filtration device and a method for separating amino acids using the filtration device. Background technique [0002] With the rapid development of the amino acid industry, my country's demand for amino acids is also increasing. At present, the main methods of artificially synthesizing amino acids include protein hydrolysis, microbial fermentation and chemical synthesis. However, most of its products are mixtures of various amino acids, which cannot be used directly. At the same time, the wastewater produced by the amino acid industry also contains a large amount of amino acid mixtures. For example, the wastewater produced by the monosodium glutamate industry contains a large amount of threonine and glutamic acid, and the wastewater pro...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01D61/14B01D67/00C07C227/40C07C229/24C07C229/26C07C229/36C07C229/08C07C229/22C07D233/64
CPCB01D61/147B01D67/0011B01D67/0016B01D67/0018B01D67/003C07C227/40C07D233/64B01D2323/46B01D2323/12C07C229/24C07C229/26C07C229/36C07C229/08C07C229/22
Inventor 谭志坚王朝云余旺易永健曾粮斌周晚来汪洪鹰杨媛茹李懋
Owner INST OF BAST FIBER CROPS CHINESE ACADEMY OF AGRI SCI