Microfiltration membrane and its preparation method and application
A technology of microfiltration membrane and membrane casting liquid, applied in the field of microfiltration membrane and its preparation, can solve the problems of low membrane pure water flux and high energy consumption equipment, and meet the requirements of high selectivity, improved water flux and energy consumption reduced effect
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[0061] The preparation method of microfiltration membrane of the present invention, comprises the steps:
[0062] S1, dissolving the polyionic liquid in an organic solvent;
[0063] S2, adding a modifying agent to the above solution for dissolution and then ultrasonically dispersing to obtain a casting solution;
[0064] S3, spreading the casting solution on a polytetrafluoroethylene plate and then drying it;
[0065] S4, soaking the polytetrafluoroethylene plate in step S3 in water, taking it out, and peeling it off to obtain a microfiltration membrane.
[0066] The organic solvent suitable for the preparation method of the present invention is not particularly limited, as long as it can dissolve the polyionic liquid. In one embodiment of the present invention, the organic solvent is N,N-dimethylformamide or dimethylsulfoxide.
[0067] In one embodiment of the present invention, the modifier is polyvinylidene fluoride.
[0068] Further, the mass fraction of polyvinylidene...
Embodiment 1
[0072] The preparation method of microfiltration membrane, comprises the steps:
[0073] S1, dissolving the polyionic liquid in N,N-dimethylformamide;
[0074] S2. Add a modifier polyvinylidene fluoride with a mass fraction of 12% to the above solution for blending, and after fully dissolving, ultrasonically remove air bubbles for 10 minutes to obtain a casting solution;
[0075] S3. After spreading the above-mentioned casting solution on the polytetrafluoroethylene board, evaporate in a blast drying oven at 80° C. for 2 hours;
[0076] S4. After immersing the polytetrafluoroethylene plate in water in step S3 to complete the phase inversion process, take it out and peel it off to obtain a microfiltration membrane.
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