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Convenient-to-clean reaction kettle for zinc sulfate production

A technology of zinc sulfate and reaction kettle, applied in the direction of zinc sulfate, chemical/physical/physical-chemical fixed reactor, cleaning hollow objects, etc., can solve problems such as unfavorable cost, increase water consumption, inconvenience, etc., and achieve convenient slag discharge and discharge, improve the effect of cleaning, improve the effect of the scope of cleaning

Inactive Publication Date: 2020-03-27
HUNAN LIHONG NEW MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, when zinc sulfate is reacted in the reactor during the preparation process, in order to improve the purity of zinc sulfate, it is generally necessary to add too much zinc powder and carry out a chemical reaction to replace all heavy metals such as copper and lead in the filtrate, as shown in the authorization announcement No. CN209138633U shows a kind of waste slag recycling device for zinc sulfate production. In the process of preparing zinc sulfate, although a device for removing and cleaning impurities is added, in this application, the inner wall of the reactor is not cleaned. Due to the mechanism, after the reaction is completed, some precipitated precipitates are attached to the inner wall. At the same time, when cleaning the kettle body, it will cause inconvenience, affect the cleaning efficiency, and increase the consumption of water resources. Conducive to cost reduction

Method used

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  • Convenient-to-clean reaction kettle for zinc sulfate production
  • Convenient-to-clean reaction kettle for zinc sulfate production
  • Convenient-to-clean reaction kettle for zinc sulfate production

Examples

Experimental program
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Effect test

Embodiment 1

[0023] The present invention provides such Figure 1-4 Shown a kind of reaction kettle that is easy to clean for the production of zinc sulfate, comprises still body 1 and the frame 2 that fixes still body 1, and described still body 1 is fixed on the upper end support plate of frame 2, and the still body 1 The crossbeam between the outer side of the bottom end and the two sets of legs of the frame 2 is fixedly connected by a fixed rod 3. The top of the kettle body 1 is equipped with a feed pipe 9, a feeding pipe 10 and a rotating shaft 4. The bottom end of the kettle body 1 is arc-shaped. Shaped setting, and a discharge port is opened in the middle position, and the discharge pipe 11 is fixedly installed on the discharge port, the rotating shaft 4 is fixedly inserted in the middle position of the kettle body 1 through the bearing, and the bottom end of the rotating shaft 4 is passed through the electric motor. The push rod 25 is connected with a bottom wiping plate 24, and th...

Embodiment 2

[0030] Specifically, two sets of heating plates 18 connected to an external power supply are installed symmetrically on the inner wall of the kettle body 1 , and the heating plates 18 may be conventional PTC heating sheets or adjustable thermostatic tubes.

[0031] Further, the stirring fan blades 16 and the nozzles 15 are arranged in a linear array on both sides of the lower end of the rotating shaft 4, and the nozzles 15 correspond to the stirring fan blades 16 alternately, wherein the inside of the nozzles 15 is also connected to the inner cavity of the rotating shaft 4 Connected, water can enter through the rotating shaft 4 and be sprayed out from the nozzle 15.

Embodiment 3

[0033] Still further, the discharge pipe 11 is a T-shaped pipe, and the top of the T-shaped is fixed and matched in the discharge port, and the two sides of the T-shaped are respectively connected with the slag discharge pipe 23 and the discharge pipe 21, and the T-shaped Valves 22 are installed on both ends, and the corresponding pipelines can be opened by controlling the valve 22 switch.

[0034] On the foregoing basis, the inside of the discharge pipe 11 is also equipped with a filter screen 26 near the inner pipe side communicating with the discharge pipe 21, and the solution discharged from the discharge pipe 21 is filtered to avoid precipitation And the unreacted zinc powder is exposed.

[0035] Concrete, this zinc sulfate production uses the reaction kettle that is easy to clean, and in use, at first dilute sulfuric acid solution is sent in the still body 1 from feeding pipe 8, and zinc powder is sent into still body 1 from feeding pipe 10, At the same time, the water pu...

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PUM

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Abstract

The invention discloses a convenient-to-clean reaction kettle for zinc sulfate production. The reaction kettle comprises a kettle body and a rack for fixing the kettle body, wherein the kettle body isfixed on a supporting plate at the upper end of the rack; the outer side of the bottom end of the kettle body is fixedly connected with a cross beam between two groups of support legs of the rack through fixing rods; a feeding pipe, an adding pipe and a rotating shaft are mounted at the top end of the kettle body; the bottom end of the kettle body is arc-shaped; a discharge port is formed in themiddle of the kettle body; a discharge pipe is fixedly mounted on the discharge port; the rotating shaft is fixedly inserted into the middle position of the kettle body through a bearing; the bottom end of the rotating shaft is connected with a bottom wiping plate through an electric push rod; stirring fan blades and nozzles are symmetrically mounted at the lower end of the rotating shaft, and cleaning assemblies are arranged at parts, on both sides of the rotating shaft, of the interior of the kettle body. According to the convenient-to-clean reaction kettle for zinc sulfate production, sediments attached to the inner wall are scraped and cleaned, and in cooperation with the nozzles mounted on the rotating shaft, when the kettle body is cleaned, scraping and water spraying can be conducted at the same time, and the cleaning effect of the reaction kettle is improved.

Description

technical field [0001] The invention belongs to the technical field of zinc sulfate production equipment, and in particular relates to an easy-to-clean reaction kettle for zinc sulfate production. Background technique [0002] Zinc sulfate, also known as alumite or zinc alumite, is a colorless or white orthorhombic crystal or powder at room temperature. It is astringent and easily soluble in water. The aqueous solution is acidic, slightly soluble in ethanol and glycerin. Pure zinc sulfate does not turn yellow when stored in the air for a long time, and loses water in dry air to form a white powder. During the production of zinc sulfate, the filtrate needs to be removed from impurities, and the filtrate needs to be sent to a replacement reactor and heated to 80°C. Add zinc powder to replace heavy metal impurities such as copper and lead, and then filter out the replacement hydraulic pressure to replace heavy metals such as copper and lead. [0003] However, when zinc sulfate...

Claims

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Application Information

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IPC IPC(8): B01J19/18B01D29/03C01G9/06B08B9/087B08B9/093
CPCB01D29/03B01J19/18B08B9/087B08B9/093C01G9/06
Inventor 张立军李才发张军
Owner HUNAN LIHONG NEW MATERIAL TECH CO LTD
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