Porous self-supporting zeolite material prepared by acid lithium slag and its preparation method and application
A technology of zeolite material and lithium slag, which is applied in the field of porous self-supporting zeolite material and its preparation, can solve the problems of high porosity, low bulk density, solid waste accumulation of lithium slag from acid process, etc., achieve excellent adsorption performance, protect the environment, protect the The effect of mechanical properties
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Embodiment 1
[0039] The preparation steps are shown in 1:
[0040] (1) Acid-process lithium slag powder (LS) is a finely ground powder obtained from the residue obtained after lithium carbonate is extracted from spodumene by sulfuric acid method. ) calcining at calcination temperature for 2h to obtain modified lithium slag powder, marked as MLS;
[0041] (2) Add 347g of alkaline activator (AA) to 400g of modified lithium slag powder and stir and mix for 2min, then add 10g of foaming agent and 2g of foam stabilizer to it, stir and mix well, then cast the mold, and then place the mold Curing in a concrete accelerated curing box at 70°C for 24 hours, the lithium slag-based geopolymer foam material was obtained, marked as FMn1.4; among them, the alkaline activator was composed of sodium hydroxide, water and water glass, and the modulus was 1.4; foaming agent is 35% mass concentration of hydrogen peroxide; foam stabilizer is analytically pure calcium stearate (Cs); the molar ratio of Na elemen...
Embodiment 2
[0044] (1) Acid-process lithium slag powder is a finely ground powder obtained by extracting lithium carbonate from spodumene by sulfuric acid method. The acid-process lithium slag powder is calcined at 700°C (heating rate 10°C / min). Calcined at lower temperature for 2 hours to obtain modified lithium slag powder, marked as MLS;
[0045] (2) Add 311g of alkaline activator to 400g of modified lithium slag powder and stir and mix for 2min, then add 15g of foaming agent and 3g of foam stabilizer to it, stir and mix well and cast the mold, then place the mold on the concrete to accelerate Curing at 70°C for 24 hours in a curing box, the lithium slag-based geopolymer foam material was obtained, which was marked as FMn1.2; among them, the alkaline activator was composed of sodium hydroxide, water and water glass, and the modulus was 1.2; The foaming agent is hydrogen peroxide with a mass concentration of 35%; the foam stabilizer is analytically pure calcium stearate; the molar ratio...
Embodiment 3
[0048] (1) Acid-process lithium slag powder is a finely ground powder obtained by extracting lithium carbonate from spodumene by sulfuric acid method. The acid-process lithium slag powder is calcined at 700°C (heating rate 10°C / min). Calcined at lower temperature for 2 hours to obtain modified lithium slag powder, marked as MLS;
[0049] (2) Add 275g of alkaline activator to 400g of modified lithium slag powder and stir and mix for 2min, then add 20g of foaming agent and 4g of foam stabilizer to it, stir and mix well and cast the mold, then place the mold on concrete to accelerate Curing in the curing box at 70°C for 24 hours, the lithium slag-based geopolymer foam material was obtained, which was marked as FMn1.0; among them, the alkaline activator was composed of sodium hydroxide, water and water glass, and the modulus was 1.0; The foaming agent is hydrogen peroxide with a mass concentration of 35%; the foam stabilizer is analytically pure calcium stearate; the molar ratio o...
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