A preparation method of nano-scale polymer electrolyte for flexible lithium battery
A lithium battery, nano-scale technology, applied in nanotechnology for materials and surface science, electrolyte storage battery manufacturing, non-aqueous electrolyte storage battery, etc., can solve multiple time, energy and electrochemical potential problems, and achieve electrochemical stability Good performance, high ionic conductivity, high thermal stability
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[0040] The present invention is further described below in conjunction with the accompanying drawings and embodiments.
[0041] The present invention proposes a method for preparing a nanoscale polymer electrolyte for a flexible lithium battery, such as Figure 1 As shown, it includes the following steps:
[0042] (1) Synthesis of crosslinked nano-polystyrene (PS).
[0043] Purified styrene is difficult to store. Commercial products often contain added inhibitors (e.g., trace amounts of hydroquinone). Pure styrene is washed with 10% NaOH solution to remove the inhibitor (tert-butyl catechol), then rinsed twice with water, and then mgSO 4 Carry out drying. Using dichloromethane as the solvent, pure styrene was separated by column chromatography. Remove the solvent and vacuum for half an hour. Pure styrene is stored at 0 °C.
[0044] Chloroform is added to vinyl anise ether, the mixture is washed with 10% sodium hydroxide, and the yellow organic matter is rinsed twice with water, wi...
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