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A kind of continuous preparation method of novel resistant dextrin dietary fiber

A technology of resistant dextrin and dietary fiber, which is applied in the field of deep processing of starch, can solve the problems of high impurities in resistant dextrin, low purity of resistant dextrin, and increased reaction liquid volume, achieving low cost and high efficiency , the effect of improving production efficiency

Active Publication Date: 2022-05-27
江苏先卓食品科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The obtained finished product of resistant dextrin contains more impurities. During the reaction process, small molecular monosaccharides, oligosaccharides and other short-chain impurities cannot be removed, and they still remain in the finished product, resulting in low purity of resistant dextrin
For example, using a tank reactor for production, the process is feed-evaporation-condensation reaction-adding water to dissolve-discharging, these four processes are carried out one by one, the second process can only be carried out after the first process is completed, although it is very It is compact, but step by step, one process at a time, is very time-consuming, and in the reaction process, due to the negative pressure evaporation and condensation reaction, it causes a lot of foam, which increases the volume of the reaction liquid, so that the amount of feed is adjusted from the volume. Therefore, the above two points lead to long reaction time, low processing capacity and low efficiency

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] (1) Sizing: glucose and isomalto-oligosaccharide are added to the water according to the ratio of 1:1 mass ratio, and then sorbitol and citric acid are added, of which the amount of sorbitol is 5% of the glucose mass ratio, the amount of citric acid is 0.3% of the glucose mass ratio, after mixing, stir evenly, heat and dissolve with water to 70% refractive, preheat to 75 ° C, to prepare the dissolved solution, to be prepared for backup;

[0028] (2) Reaction: open the scraper evaporator electric heating switch, heat up the heat transfer oil to 160 ° C, open the heat conduction oil circulation pump, preheat the scraper evaporator, preheat to the jacket temperature to 158 ° C, open the vacuum pump, to the vacuum degree -0.084Mpa, open the scraper evaporator feed pump, the dissolved liquid from the upper part of the scraper evaporator to start feeding, feed flow 1.5 square / h (dry base), the dissolved liquid through the scraper evaporator, the upper half is the evaporation sect...

Embodiment 2

[0033] (1) Sizing: add glucose and isomalto-oligosaccharide to water in accordance with the ratio of 2:1 mass ratio, and then add sorbitol and citric acid, of which the amount of sorbitol is 8% of the glucose mass ratio, the amount of citric acid added is 0.7% of the glucose mass ratio, mixed evenly, heated and dissolved with water to 78% refractive, preheated to 77 ° C, to prepare the dissolved solution, to be prepared;

[0034](2) Reaction: open the scraper evaporator electric heating switch, heat up the heat transfer oil to 180 ° C, open the heat conduction oil circulation pump, preheat the scraper evaporator, preheat to the jacket temperature to 179 ° C, open the vacuum pump, to the vacuum degree -0.084Mpa, open the scraper evaporator feed pump, the dissolved liquid from the upper part of the scraper evaporator to start feeding, feed flow 1.75 square / h (dry base), the dissolved liquid through the scraper evaporator, the upper half is the evaporation section, the lower half i...

Embodiment 3

[0039] (1) Sizing: add glucose and isomalto-oligosaccharide to water according to the ratio of mass ratio of 1.5:1, and then add sorbitol and citric acid, of which the amount of sorbitol is 8% of the glucose mass ratio, the amount of citric acid is 0.7% of the glucose mass ratio, after mixing, stir evenly, heat and dissolve with water to 78% refractive, preheat to 77 ° C, prepare the dissolved solution, to be prepared for backup;

[0040](2) Reaction: open the scraper evaporator electric heating switch, heat up the heat transfer oil to 185 ° C, open the heat conduction oil circulation pump, preheat the scraper evaporator, preheat to the jacket temperature to 183 ° C, open the vacuum pump, to the vacuum degree -0.084Mpa, open the scraper evaporator feed pump, the dissolved liquid from the upper part of the scraper evaporator to start feeding, feed flow 2.0 square / hour (dry base), the dissolved liquid through the scraper evaporator, the upper half is the evaporation section, the l...

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Abstract

The invention discloses a continuous preparation method of novel resistant dextrin dietary fiber, comprising the following steps: dissolving glucose and isomaltooligosaccharide in water, adding sorbitol and citric acid, stirring evenly, heating and dissolving to obtain a solution; The prepared solution is injected from the upper part of the scraper evaporator into a scraper evaporator with a preheating temperature of 160-190°C and a vacuum degree of -0.084MPa or above for reaction, and the solution is condensed to obtain a condensate in a molten state ;Put the condensate in water for activated carbon decolorization to obtain a reaction solution; perform ion exchange on the reaction solution, and finally separate the membrane to separate and concentrate the ion-exchange solution to obtain a concentrated solution, which is spray-dried or evaporated to obtain a resistant dextrin with a content greater than or equal to 84%. Dietary fiber. The invention integrates evaporation, condensation reaction, dissolution, and feeding into one, and is carried out simultaneously without mutual interference, so as to achieve the purpose of continuous production, and the method has low energy consumption, simple operation, high yield and low cost.

Description

Technical field [0001] The present invention relates to the field of starch deep processing technology, specifically to a new type of resistant dextrin dietary fiber continuous preparation method. Background [0002] Resistant dextrin, an important product of starch deep processing, is a low-calorie dextran, which belongs to the low molecular weight soluble dietary fiber, dietary fiber is known as the seventh major nutrient necessary for human health, and is an important raw material for the modern food industry. Resistant dextrins are one of the "low viscosity water-soluble dietary fibers", low viscosity, low calorie, low sweetness, high solubility and good processing stability. Because it contains indigestible components that are resistant to the role of human digestive enzymes (amylase, glucose amylase, etc.), it will not be digested and absorbed in the digestive tract, and can directly enter the large intestine, promote the growth of beneficial bifidobacteria and lactic acid ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08B37/00
CPCC08B37/006
Inventor 韩承勇刘峰韩先卓钟礼杰
Owner 江苏先卓食品科技股份有限公司