Three-channel efficient continuous flow photochemical mixing device and mixing method thereof
A mixing device and photochemical technology, applied in the field of flow photochemistry, can solve the problems of difficult mixing effect, time-consuming, local overheating danger, etc., and achieve the effects of reducing potential safety hazards, improving multi-step synthesis, providing mixing effect and heat transfer efficiency
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Embodiment 1
[0057] See attached figure 1 And attached figure 2 , the embodiment of the present invention discloses a three-channel high-efficiency continuous flow photochemical mixing device, comprising: an injection assembly 1, a first reaction assembly 2, a first Y-shaped pipeline 3, a second reaction assembly 4, a second Y-shaped pipeline 5 and collection container 6;
[0058]The injection assembly 1 includes three injection pumps 11, and syringes 12 respectively installed on the injection pumps 11;
[0059] The first reaction assembly 2 includes a first carrier 21, and a first reaction pipeline 22 spirally wound and fixed on the outer wall of the first carrier 21;
[0060] Two openings in the first Y-shaped pipeline 3 communicate with the injection ports of the two syringes 12 respectively, and the other opening communicates with the inlet of the first reaction pipeline 22;
[0061] The second reaction assembly 4 includes a second carrier 41, and a second reaction pipeline 42 spir...
Embodiment 2
[0071] The embodiment of the present invention discloses a mixing method of a three-channel high-efficiency continuous flow photochemical mixing device, comprising the following steps:
[0072] S1. According to different mixing requirements, set different driving flow rates for the syringe pump 11;
[0073] S2. First start the two syringe pumps 11 connected to the first Y-shaped pipeline 3, so that two different materials are pushed out from the two syringes 12, flow through the first Y-shaped pipeline 3 and then pass through the first reaction pipeline 22 The inlet enters the spiral flow mixing in the first reaction pipeline 22, and enters the second Y-shaped pipeline 5 from the outlet of the first reaction pipeline 22;
[0074] S3. Start the syringe pump 11 connected to the second Y-shaped pipeline 5, so that the third material is pushed out from the syringe 12, flows through the second Y-shaped pipeline 5 and the mixed material in S2 converges again, and passes through the ...
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