A kind of preparation method of high-performance modified polyimide flexible composite film
A polyimide flexible and polyimide technology, which is applied in the field of preparation of high-performance modified polyimide flexible composite films, can solve the problem of high dielectric loss and moisture absorption, inability to ultra-thin film, preparation Complex process and other problems, to achieve good high-voltage insulation, mechanical strength and toughness, ensure cohesion and high stickiness, and simple preparation process.
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Embodiment 1
[0040] A preparation method of a high-performance modified polyimide flexible composite film, comprising the following steps:
[0041] Step 1: Add the modified polyimide (MPI) glue, antioxidant, toughening agent, curing agent, anti-aging agent and flame retardant to the mixed solvent of methyl ethyl ketone and xylene, after pretreatment and grinding It is formulated into MPI glue; the pretreatment is distillation pretreatment;
[0042] Step 2: Coat the MPI glue obtained in step 1 on a PI film with a thickness of 0.005mm, with a coating thickness of 0.001mm, and then enter a tunnel oven at a temperature of 60°C at a line speed of 5m / min for drying and pre-curing, so that the The glue becomes a pre-cured adhesive layer, and the release film / paper is applied at 180°C and 0.005MPa to obtain a single-sided semi-cured MPI adhesive layer composite film. The single-sided semi-cured MPI adhesive layer composite film includes a semi-cured adhesive layer and a film. Floor;
[0043] Ste...
Embodiment 2
[0046] A preparation method of a high-performance modified polyimide flexible composite film, comprising the following steps:
[0047] Step 1: Add the modified polyimide (MPI) glue and antioxidants, toughening agents, stabilizers, and plasticizers to a mixed solvent of N-methylpyrrolidone (NMP), methanol and chloroform, and pass MPI glue is prepared after pretreatment and grinding; the pretreatment is stirring pretreatment;
[0048] Step 2: Coat the MPI glue obtained in Step 1 on a PET film with a thickness of 0.3 mm, with a coating thickness of 3 mm, and then enter a tunnel oven at a temperature of 200 ° C at a line speed of 40 m / min for drying and pre-curing to make the glue It becomes a pre-cured adhesive layer, and the release film / paper is applied at 25°C and 0.5MPa to obtain a single-sided semi-cured MPI adhesive layer composite film. The single-sided semi-cured MPI adhesive layer composite film includes a semi-cured adhesive layer and a film layer. ;
[0049] Step 3: ...
Embodiment 3
[0053] A preparation method of a high-performance modified polyimide flexible composite film, comprising the following steps:
[0054] Step 1: Add modified polyimide (MPI) glue and stabilizer, plasticizer, UV absorber to N,N-dimethylformamide (DMF), phenol, cyclohexanone and chloroform MPI glue is prepared in the mixed solvent after pretreatment and grinding; the pretreatment is preheating pretreatment;
[0055] Step 2: Coat the MPI glue obtained in step 1 on the LCP film with a thickness of 0.025mm, and the coating thickness is 0.010mm, and then enter a tunnel oven at a temperature of 180°C at a line speed of 30m / min for drying and pre-curing, so that the The glue becomes a pre-cured adhesive layer, and the release film / paper is applied at 80°C and 0.075MPa to obtain a single-sided semi-cured MPI adhesive layer composite film. The single-sided semi-cured MPI adhesive layer composite film includes a semi-cured adhesive layer and a film. Floor;
[0056] Step 3: Preheat the si...
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