Preparation method of high-performance modified polyimide (MPI) flexible substrate
A polyimide flexible and high-performance technology, applied in chemical instruments and methods, flat products, film/sheet adhesives, etc., can solve the problem of high dielectric loss and high moisture absorption, which cannot meet high-voltage insulation With high current carrying requirements, easy breakage and bendability, etc., it achieves good high-voltage insulation, mechanical strength and toughness, meets the process window and low-cost production, and improves high temperature resistance and stickiness.
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Embodiment 1
[0040] A method for preparing a high-performance modified polyimide flexible substrate, comprising the steps of:
[0041] Step 1: Add the modified polyimide (MPI) glue and antioxidant, toughening agent, curing agent, antiaging agent and flame retardant to the mixed solvent of butanone and xylene, after pretreatment and grinding Prepared as MPI glue; the pretreatment is distillation pretreatment;
[0042] Step 2: Coat the MPI glue obtained in step 1 on a copper foil with a thickness of 0.005mm, and the thickness of the coating is 0.001mm, and then enter the tunnel oven at a temperature of 80°C at a line speed of 1m / min to dry and pre-cure, so that The glue becomes a pre-cured adhesive layer, and the release film / paper is applied at 320°C and 0.06MPa to obtain a single-sided semi-cured MPI adhesive-layer substrate, which includes a semi-cured adhesive layer and a foil layer;
[0043] Step 3: Unwind the single-sided semi-cured MPI adhesive layer substrate obtained in step 2 and ...
Embodiment 2
[0046] A method for preparing a high-performance modified polyimide flexible substrate, comprising the steps of:
[0047] Step 1: Add modified polyimide (MPI) glue and antioxidant, toughening agent, stabilizer, plasticizer to N-methylpyrrolidone (NMP), in the mixed solvent of methyl alcohol and chloroform, through Prepare MPI glue after pretreatment and grinding; the pretreatment is stirring pretreatment;
[0048] Step 2: Coat the MPI glue obtained in step 1 on a silver foil with a thickness of 0.5mm, and the coating thickness is 3mm, and then enter a tunnel oven at a temperature of 280°C at a line speed of 26m / min for drying and pre-curing, so that the glue Become a pre-cured adhesive layer, apply a release film / paper at 60°C and 10MPa to obtain a single-sided semi-cured MPI adhesive-line substrate, and the single-sided semi-cured MPI adhesive-line substrate includes a semi-cured adhesive layer and a foil layer;
[0049] Step 3: Preheat the single-sided semi-cured MPI adhesi...
Embodiment 3
[0053] A method for preparing a high-performance modified polyimide flexible substrate, comprising the steps of:
[0054] Step 1: Add modified polyimide (MPI) glue and stabilizer, plasticizer, UV absorber to N,N-dimethylformamide (DMF), phenol, cyclohexanone and chloroform In the mixed solvent, it is prepared into MPI glue after pretreatment and grinding; the pretreatment is preheating pretreatment;
[0055] Step 2: Coat the MPI glue obtained in step 1 on an aluminum foil with a thickness of 0.025mm, and the coating thickness is 0.010mm, and then enter a tunnel oven at a temperature of 200°C at a line speed of 20m / min to dry and pre-cure, so that the glue Become a pre-cured adhesive layer, apply a release film / paper at 200°C and 0.175MPa to obtain a single-sided semi-cured MPI adhesive-line substrate, and the single-sided semi-cured MPI adhesive-line substrate includes a semi-cured adhesive layer and a foil layer;
[0056] Step 3: Preheat the single-sided semi-cured MPI adhes...
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