A preparation method of high-performance modified polyimide flexible substrate
A polyimide flexible and polyimide technology is applied in the field of preparation of high-performance modified polyimide flexible substrates, and can solve the problem of high dielectric loss and moisture absorption, complex preparation process and mechanical strength. and insufficient toughness, to achieve good high-voltage insulation, mechanical strength and toughness, simple preparation process, and ensure the effect of stickiness
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Embodiment 1
[0040] A preparation method of a high-performance modified polyimide flexible substrate, comprising the following steps:
[0041] Step 1: Add the modified polyimide (MPI) glue, antioxidant, toughening agent, curing agent, anti-aging agent and flame retardant to the mixed solvent of methyl ethyl ketone and xylene, after pretreatment and grinding It is formulated into MPI glue; the pretreatment is distillation pretreatment;
[0042] Step 2: Coat the MPI glue obtained in step 1 on a copper foil with a thickness of 0.005mm, and the coating thickness is 0.001mm, and then enter the tunnel oven at a temperature of 1m / min to dry and pre-cure it at a temperature of 80°C. The glue becomes a pre-cured adhesive layer, and the release film / paper is applied at 320° C. and 0.06 MPa to obtain a single-sided semi-cured MPI adhesive layer substrate. The single-sided semi-cured MPI adhesive layer substrate includes a semi-cured adhesive layer and a foil layer;
[0043] Step 3: Unwind the single...
Embodiment 2
[0046] A preparation method of a high-performance modified polyimide flexible substrate, comprising the following steps:
[0047] Step 1: Add the modified polyimide (MPI) glue and antioxidants, toughening agents, stabilizers, and plasticizers to a mixed solvent of N-methylpyrrolidone (NMP), methanol and chloroform, and pass MPI glue is prepared after pretreatment and grinding; the pretreatment is stirring pretreatment;
[0048] Step 2: Coat the MPI glue obtained in Step 1 on a silver foil with a thickness of 0.5mm, with a coating thickness of 3mm, and then enter a tunnel oven at a temperature of 280°C at a line speed of 26m / min for drying and pre-curing to make the glue It becomes a pre-cured adhesive layer, and the release film / paper is applied at 60°C and 10MPa to obtain a single-sided semi-cured MPI adhesive layer substrate, and the single-sided semi-cured MPI adhesive layer substrate includes a semi-cured adhesive layer and a foil layer;
[0049] Step 3: Preheat the singl...
Embodiment 3
[0053] A preparation method of a high-performance modified polyimide flexible substrate, comprising the following steps:
[0054] Step 1: Add modified polyimide (MPI) glue and stabilizer, plasticizer, UV absorber to N,N-dimethylformamide (DMF), phenol, cyclohexanone and chloroform MPI glue is prepared in the mixed solvent after pretreatment and grinding; the pretreatment is preheating pretreatment;
[0055] Step 2: Coat the MPI glue obtained in Step 1 on an aluminum foil with a thickness of 0.025mm, and the coating thickness is 0.010mm, and then enter a tunnel oven at a temperature of 200 m / min at a line speed of 20m / min for drying and pre-curing to make the glue It becomes a pre-cured adhesive layer, and the release film / paper is applied at 200°C and 0.175MPa to obtain a single-sided semi-cured MPI adhesive layer substrate, and the single-sided semi-cured MPI adhesive layer substrate includes a semi-cured adhesive layer and a foil layer;
[0056] Step 3: Preheat the single-s...
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