High-adsorbability resin and preparation method thereof

A high adsorption, resin technology, applied in separation methods, chemical instruments and methods, solid adsorbent liquid separation, etc., can solve the problems of short service life of activated carbon, low capacity of activated carbon adsorption method, etc., and achieve fast adsorption process and regeneration method. Simple, repeatable effects

Active Publication Date: 2020-11-20
谦信化工集团有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

At present, traditional methods are mainly used for the disposal of such oily pollutants, such as activated carbon adsorption, biodegradation, flocculation, or the use of oil dispersants. Among them, activated carbon is widely used, but the capacity of activated carbon adsorption is low. short service life

Method used

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  • High-adsorbability resin and preparation method thereof
  • High-adsorbability resin and preparation method thereof

Examples

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Embodiment 1

[0022] An embodiment of the highly absorbent resin of the present invention, the highly absorbent resin described in this embodiment comprises the following raw material components in parts by weight: 10 parts of water, 22 parts of butyl methacrylate, 10 parts of sodium acrylate, 35 parts butyl acrylate, 20 parts styrene, 1 part sodium lauryl sulfate, 4 parts n-pentane, and 0.8 parts benzoyl peroxide.

[0023] The preparation method of the highly absorbent resin described in this embodiment comprises the following steps: (1) mix butyl methacrylate, sodium acrylate, butyl acrylate, styrene and sodium lauryl sulfate, add water and heat to 40 After dissolving at ℃, cool to obtain a clear solution; (2) add n-pentane and benzoyl peroxide to the clear solution obtained in step (1) and stir to dissolve, first raise the temperature to 55°C and keep it warm for 1.5h, then raise the temperature to 70°C ℃ and keep it warm for 2 hours, and finally raise the temperature to 85 ℃ and keep it...

Embodiment 2

[0025] An embodiment of the highly absorbent resin of the present invention, the highly absorbent resin described in this embodiment comprises the following raw material components in parts by weight: 15 parts of water, 19 parts of lauryl methacrylate, 5 parts of sodium acrylate, 40 parts butyl acrylate, 20 parts styrene, 1 part sodium lauryl sulfate, 4 parts n-pentane, and 0.8 parts benzoyl peroxide.

[0026] The preparation method of the highly absorbent resin described in this embodiment comprises the following steps: (1) mixing lauryl methacrylate, sodium acrylate, butyl acrylate, styrene and sodium lauryl sulfate, adding water and heating to After dissolving at 40°C, cool to obtain a clear solution; (2) Add n-pentane and benzoyl peroxide to the clear solution obtained in step (1) and stir to dissolve, then raise the temperature to 60°C and keep it warm for 1 hour, then raise the temperature to 70°C °C and keep it warm for 1.5h, and finally raise the temperature to 90°C an...

Embodiment 3

[0028] An embodiment of the highly absorbent resin of the present invention, the high absorbent resin described in this embodiment comprises the following raw material components in parts by weight: 14 parts of water, 15 parts of butyl methacrylate, 5 parts of sodium acrylate, 40 2-ethylhexyl acrylate, 25 parts styrene, 1 part sodium oleate, 1 part cyclohexane, and 1 part azobisisobutyronitrile.

[0029] The preparation method of the highly absorbent resin described in this embodiment comprises the following steps: (1) mixing butyl methacrylate, sodium acrylate, 2-ethylhexyl acrylate, styrene and sodium oleate, adding water and After heating to 40°C to dissolve, cool to obtain a clear solution; (2) add cyclohexane and azobisisobutyronitrile to the clear solution obtained in step (1) and stir to dissolve, then raise the temperature to 60°C and keep it warm for 0.5h, Then raise the temperature to 70° C. and keep it warm for 2 hours, and finally raise the temperature to 90° C. an...

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Abstract

The invention discloses high-adsorbability resin which comprises the following raw material components in parts by weight: 1-15 parts of water, 15-30 parts of methacrylate, 5-15 parts of acrylate, 15-50 parts of acrylate and 10-30 parts of styrene. The high-adsorbability resin also comprises a pore-foaming agent and an initiator. The product is stable in polarity, easy to store and moderate in viscosity, has the advantages of being high in adsorption rate, high in adsorption capacity, good in mechanical strength, simple in regeneration mode and the like, and can effectively adsorb an organic poison solvent and solve the leakage problem of the organic poison solvent. The invention further discloses a preparation method of the high-adsorbability resin. The preparation method is simple to operate, safe in preparation process, free of by-products, high in repeatability and beneficial to large-scale preparation. The invention also discloses an application of the high-adsorbability resin inorganic poison adsorption. The product can be used for adsorption treatment of organic toxicants such as acetic acid short-chain ester, benzene compounds and chlorides.

Description

technical field [0001] The invention belongs to the field of adsorption resins, and in particular relates to a highly absorbent resin and a preparation method thereof. Background technique [0002] With the rapid development of my country's social economy and chemical industry, the scope of application of chemicals has become more and more extensive. At the same time, environmental pollution caused by oily sewage, waste liquids and industrial accidents such as the leakage of ethyl acetate has become increasingly serious. At present, traditional methods are mainly used for the disposal of such oily pollutants, such as activated carbon adsorption, biodegradation, flocculation, or the use of oil dispersants. Among them, activated carbon is widely used, but the capacity of activated carbon adsorption is low. Short service life. Compared with these traditional treatment methods for low-viscosity oils, super oil-absorbing resins can modify polymer resins according to the types of...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J20/26B01J20/30B01D15/00C08F220/18C08F212/08C08F220/06C08F220/14C08J9/14C08L33/08C08L25/14
CPCB01J20/264B01D15/00C08F220/1804C08F220/1808C08F212/08C08J9/141C08J2333/08C08J2203/14C08J2325/14C08F220/1812C08F220/06C08F220/14
Inventor 钟慧娴李庭忠佟刚
Owner 谦信化工集团有限公司
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