Preparation method of microcrystal foam thermal insulation decorative plate through lithium deposition sintering
A technology for thermal insulation decorative panels and microcrystals, which is applied in glass manufacturing equipment, manufacturing tools, glass molding, etc., can solve the problems of insufficient environmental protection in the production and processing of thermal insulation decorative panels, and low recycling and utilization of lithium precipitation mother liquor, so as to achieve outstanding use value, The effect of reducing economic losses
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Embodiment 1
[0022] The present invention provides a technical solution: a preparation method for sintering microcrystalline foam thermal insulation decorative board by lithium deposition, which includes the following steps in sequence:
[0023] (1) Treatment of lithium sinking mother liquor: Add concentrated sulfuric acid with a mass fraction of 98% to the lithium sinking mother liquor until the pH of the mixed solution is 3-7, then continuously monitor the pH of the solution and maintain the pH of the mixed solution at 3-7 by controlling the amount of sulfuric acid added ; Pass the mixed solution through the NF membrane and the RO membrane in turn, collect the intercepted solution at the front end of the membrane respectively, and re-mix the intercepted solution into the lithium sinking mother liquor; repeat the above process, and collect a high-concentration lithium ion solution at the front end of the NF membrane and the RO membrane, Lithium sinking mother liquor refers to the lithium s...
Embodiment 2
[0032] The present invention provides a technical solution: a preparation method for sintering microcrystalline foam thermal insulation decorative board by lithium deposition, which includes the following steps in sequence:
[0033] (1) Treatment of lithium sinking mother liquor: add concentrated sulfuric acid with a mass fraction of 98% to the lithium sinking mother liquor until the pH of the mixed solution is at 3, then continuously monitor the pH of the solution and maintain the pH of the mixed solution at 3 by controlling the amount of sulfuric acid added; Through the NF membrane and the RO membrane in turn, the intercepted solution at the front end of the membrane is collected respectively, and the intercepted solution is re-mixed into the lithium sinking mother solution; the above process is repeated, and a high-concentration lithium ion solution is collected at the front end of the NF membrane and the RO membrane, and the lithium sinking mother solution is Refers to the ...
Embodiment 3
[0042] The present invention provides a technical solution: a preparation method for sintering microcrystalline foam thermal insulation decorative board by lithium deposition, which is characterized in that it includes the following steps in sequence:
[0043] (1) Treatment of lithium sinking mother liquor: Add concentrated sulfuric acid with a mass fraction of 98% to the lithium sinking mother liquor until the pH of the mixed solution is 5, then continuously monitor the pH of the solution and maintain the pH of the mixed solution at 5 by controlling the amount of sulfuric acid added; Through the NF membrane and the RO membrane in turn, the intercepted solution at the front end of the membrane is collected respectively, and the intercepted solution is remixed into the lithium sinking mother solution; the above process is repeated, and a high-concentration lithium ion solution is collected at the front end of the NF membrane and the RO membrane. The lithium sinking mother solutio...
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