Catalyst for preparing o-toluidine by hydrogenating o-nitrotoluene and preparation method of catalyst
A technology for o-nitrotoluene and o-toluidine is applied in the field of catalytic hydrogenation of o-nitrotoluene to prepare o-toluidine catalyst and the field of preparation thereof, and can solve the problems of easy crushing selectivity, poor thermal stability, low temperature and the like
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Embodiment 1
[0035] (1) Weigh 100g of raw silica gel and wash it with deionized water, put it into a reactor equipped with 200ml of deionized water, control the temperature of the reactor at 130°C, and the reaction pressure at 0.35MPa, and add concentrated nitric acid to adjust the solution under stirring conditions The acidity, adjust the concentration of nitric acid solution to 3%, the treatment time is 2h, and then wash with deionized water until the pH value of the washing solution is 7.0; (2) Weigh 100g copper nitrate and dissolve it in 180ml deionized water, the pH value of the solution is 5 , adding ammonia water with a specific gravity of 0.985 to the copper nitrate solution, controlling the pH value of the solution to be 10, forming a molecular formula of [Cu(NH 3 ) 4 ] 2+ copper ammonia complex, the copper content in the complex is 30g / l; (3) Add the copper ammonia complex obtained in step (2) into the dipping kettle, and add the modified silica gel obtained in step (1) Among t...
Embodiment 2
[0037](1) Weigh 100g of raw silica gel and wash it with deionized water, put it into a reactor equipped with 200ml of deionized water, control the temperature of the reactor at 140°C, and the reaction pressure at 0.25MPa, and add concentrated nitric acid to adjust the solution under stirring conditions The acidity, adjust the concentration of nitric acid solution to 4%, the treatment time is 2.5h, and then wash with deionized water until the pH value of the washing solution is 7.0; (2) Weigh 100g of copper nitrate and dissolve it in 180ml of deionized water, the pH of the solution is 4. Add ammonia water with a specific gravity of 0.985 to the copper nitrate solution, control the pH value of the solution to 9, and form a molecular formula of [Cu(NH 3 ) 4 ] 2+ copper ammonia complex, the copper content in the complex is 32g / l; (3) Add the copper ammonia complex obtained in step (2) into the dipping kettle, and add the modified silica gel obtained in step (1) Among them, at a ...
Embodiment 3
[0039] (1) Weigh 100g of raw silica gel and wash it with deionized water, put it into a reactor equipped with 200ml of deionized water, control the temperature of the reactor at 135°C, and the reaction pressure at 0.3MPa, and add concentrated nitric acid to adjust the solution under stirring conditions The acidity, adjust the concentration of nitric acid solution to 4%, the treatment time is 3h, and then wash with deionized water until the pH value of the washing solution is 7.0; (2) Weigh 100g copper nitrate and dissolve it in 180ml deionized water, the pH value of the solution is 6 , adding ammonia water with a specific gravity of 0.984 to the copper nitrate solution, controlling the pH of the solution to be 11, forming a molecular formula of [Cu(NH 3 ) 4 ] 2+ copper ammonia complex, the copper content in the complex is 35g / l; (3) Add the copper ammonia complex obtained in step (2) into the dipping kettle, and add the modified silica gel obtained in step (1) Among them, at...
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Abstract
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