Method of controlling production of excess water and aqueous fluids in oil and gas wells
A water-based fluid and water-soluble salt technology, applied in chemical instruments and methods, drilling compositions, etc., can solve the problems of difficult recovery operations and increased operating costs.
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example 1-
[0264] Example 1 - Preparation of active ionic polymer dispersants (first step (i))
[0265] The polymer dispersant was prepared according to the following procedure: 250.03 g of 2-acrylamide-2-methylpropanesulfonic acid sodium salt (50 wt %), 0.05 g of A1 (radical polymerization control agent, purchased from Solvay) and 250.11 g of deionized water were injected into a 1-liter reactor equipped with a mechanical stirrer, and the mixture was stirred at 200 rpm for 30 minutes to form a homogeneous solution. The solution was first bubbled with 800cc / min nitrogen for 40 minutes, then heated to 35°C, and then added 0.5g of 5wt% sodium persulfate (SPS) aqueous solution and 1.3g of 5wt% sodium formaldehyde sulfoxylate (NaFS ) aqueous solution. After every hour, the same amount of SPS and NaFS was added. After 3 hours, the resulting viscous solution was heated to 45-50°C and 0.5 g of a 10 wt% solution of 2,2'-azobis(2-methylpropionamide) dihydrochloride was added. After aging for 1...
example 2
[0266] Example 2 - Preparation of polymer emulsion (second step (ii))
[0267] 71.66 g of ammonium sulfate, 12.58 g of sodium sulfate, 0.05 g of EDTA, and 213.2 g of deionized water were injected into a 1 liter resin reactor and stirred for 15 minutes. Subsequently, 95.12 g of acrylamide (50 wt %), 8.6 g of glycerol, 53.09 g of sodium 2-acrylamide-2-methylpropanesulfonate (50 wt %) and 44.6 g of the polymer prepared in Example 1 were added Disperse and stir to form a homogeneous solution. The solution was sparged with 800 cc / min of nitrogen for 40 minutes, then heated to 40° C., followed by the addition of 0.75 g of a 10 wt % aqueous solution of 2,2′-azobis(2-methylpropionamide) dihydrochloride . After every 30 minutes, an equal amount of 2,2'-azobis(2-methylpropionamide) dihydrochloride was added. During the polymerization, the whole mixture became milky. After 3 hours, 3 g of 10 wt % 2,2'-azobis(2-methylpropionamide) dihydrochloride solution was added and aged for 1 hour...
example 3
[0268] Example 3 - Preparation of polymer emulsion (second step (ii))
[0269] 71.65 g of ammonium sulfate, 12.61 g of sodium sulfate, 0.05 g of EDTA, and 213.0 g of deionized water were injected into a 1 liter resin reactor and stirred for 15 minutes. Subsequently, 118.45 g of acrylamide (50 wt %), 4.3 g of glycerin, 29.59 g of sodium 2-acrylamide-2-methylpropanesulfonate (50 wt %) and 44.63 g of the polymer prepared in Example 1 were added Disperse and stir to form a homogeneous solution. The solution was sparged with 800 cc / min of nitrogen for 40 minutes, then heated to 40° C., followed by the addition of 0.75 g of a 10 wt % aqueous solution of 2,2′-azobis(2-methylpropionamide) dihydrochloride . After every 30 minutes, an equal amount of 2,2'-azobis(2-methylpropionamide) dihydrochloride was added. During the polymerization, the whole mixture became milky. After 3 hours, 3 g of 10 wt % 2,2'-azobis(2-methylpropionamide) dihydrochloride solution was added and aged for 1 ho...
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