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Al-V intermediate alloy for aluminum and preparation method thereof

A master alloy, vanadium-aluminum alloy technology, applied in the field of metallurgy technology and metal materials, can solve the problem that the type of V phase cannot be accurately controlled

Pending Publication Date: 2022-04-29
NORTH CHINA UNIVERSITY OF TECHNOLOGY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] In view of the problem that the existing Al-V master alloy for aluminum cannot be precisely controlled in the type of V phase, the present invention provides an Al-V master alloy for aluminum and a preparation method thereof

Method used

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  • Al-V intermediate alloy for aluminum and preparation method thereof
  • Al-V intermediate alloy for aluminum and preparation method thereof
  • Al-V intermediate alloy for aluminum and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0043] (1) select a pure aluminum block with a purity of 99.9%, place it in a graphite clay crucible and melt it in a well-type resistance furnace;

[0044] (2) Proportionally weighing vanadium-aluminum alloy particles containing V (percentage by weight) is 50%, so that the weight ratio of vanadium-aluminum alloy and pure aluminum block is 2:23;

[0045] (3) After heating the pure aluminum melt to 850°C, adding vanadium-aluminum alloy particles, the size of the added vanadium-aluminum alloy particles is 3-5 mm;

[0046] (4) Pass argon protection into the furnace, and raise the temperature to 1150°C within 30 minutes, and use a hand-held graphite rod to stir the alloy melt clockwise until no particle movement at the bottom of the furnace is felt.

[0047] (5) Insulate at 1150° C. for 10 minutes, and at the same time continue to feed argon protective gas into the furnace, and stir once for 5 minutes and 10 minutes respectively with a graphite stirring paddle, each stirring time ...

Embodiment 2

[0051] The specific method is the same as in Example 1, except that the cooling rate corresponding to the solidification of the water-cooled copper mold in step (6) is 880° C. / s. In the Al-V master alloy for aluminum obtained in this embodiment, V is 3.98% by weight, Fe is 0.11%, and the balance is Al and impurities.

[0052] The microstructure of the Al-V master alloy for aluminum obtained in Example 2 is observed, and the results are shown in figure 2 . It can be seen that the V-containing phases in the alloy structure are all Al 10 V phase, the content is 23.8%, and Al 10 V-phase size is very small.

Embodiment 3

[0054] The specific method is the same as in Example 1, except that the casting mold in step (6) is a refractory material mold, and the corresponding solidification cooling rate is 2.4° C. / s. In the Al-V master alloy for aluminum obtained in this embodiment, V is 4.02% by weight, Fe is 0.14%, and the balance is Al and impurities.

[0055] The microstructure of the Al-V master alloy for aluminum obtained in Example 3 is observed, and the results are shown in image 3 . It can be seen that the V-containing phase in the alloy structure is a large amount of Al 10 V phase and a very small amount of Al 3 V phase, Al 10 V phase and Al 3 The content of V phase is 30.4% and 1.4%, respectively, and Al 10 V phase and Al 3 The V phases are all very thick in size.

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Abstract

The invention discloses an Al-V intermediate alloy for aluminum and a preparation method of the Al-V intermediate alloy, and belongs to the technical field of metallurgical technologies and metal materials, the Al-V intermediate alloy for aluminum comprises the following components in percentage by weight: 3-6% of V, less than or equal to 0.2% of Fe, and the balance of Al and impurities. The V-containing phase type and content in the microstructure of the Al-V intermediate alloy for aluminum can be accurately controlled, and the Al-V intermediate alloy for aluminum is suitable for various quality and requirements and is applied to commercial aluminum alloy smelting so as to meet different requirements of industrial production.

Description

technical field [0001] The invention relates to the fields of metallurgy technology and metal material technology, in particular to an Al-V master alloy for aluminum and a preparation method thereof. Background technique [0002] The trace addition of alloying element vanadium (V) in commercial aluminum alloys is usually realized in the form of Al-V master alloys for aluminum. Using the Al-V master alloy for aluminum, the successful addition of V elements in commercial aluminum alloys can be achieved through conventional commercial aluminum alloy smelting methods. [0003] However, since the types of V-containing phases formed by V and Al are not unique, the types and contents of V-containing phases in Al-V master alloys for aluminum obtained under different preparation process conditions vary widely. [0004] At present, the preparation technology for obtaining accurate, stable and uniform Al-V master alloys with V content is relatively mature, but a large number of techno...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C21/00C22C1/03B22D27/04
CPCC22C21/00C22C1/026C22C1/03B22D27/04
Inventor 蒙毅杨越曹雷刚李岑刘霄壤
Owner NORTH CHINA UNIVERSITY OF TECHNOLOGY